Technology Process of C43H47O11N5S
There total 10 articles about C43H47O11N5S which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetrabutyl ammonium fluoride;
In
tetrahydrofuran;
at 20 ℃;
for 1h;
DOI:10.1021/ol070990u
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 90 percent / triethylamine; DMAP; pyridine / 6 h / 20 °C
2: 90 percent / H2 / Pd/C / methanol / 3.5 h / 2068.65 Torr
3: 78 percent / HBTU; DIPEA; HOBt / acetonitrile / 1 h / 20 °C
4: 90 percent / TBAF / tetrahydrofuran / 1 h / 20 °C
With
pyridine; dmap; tetrabutyl ammonium fluoride; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/ol070990u
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 90 percent / triethylamine; DMAP; pyridine / 6 h / 20 °C
2: 90 percent / H2 / Pd/C / methanol / 3.5 h / 2068.65 Torr
3: 78 percent / HBTU; DIPEA; HOBt / acetonitrile / 1 h / 20 °C
4: 90 percent / TBAF / tetrahydrofuran / 1 h / 20 °C
With
pyridine; dmap; tetrabutyl ammonium fluoride; hydrogen; benzotriazol-1-ol; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; triethylamine; N-ethyl-N,N-diisopropylamine;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; acetonitrile;
DOI:10.1021/ol070990u
