(R)-3-[4-(2-allyl-6-nitro-2,3-dihydro-imidazo[2,1-b]oxazol-2-yl)-phenyl]-5-hydroxymethyl-oxazolidin-2-one

Base Information

Chemical Name:(R)-3-[4-(2-allyl-6-nitro-2,3-dihydro-imidazo[2,1-b]oxazol-2-yl)-phenyl]-5-hydroxymethyl-oxazolidin-2-one
CAS No.:1188918-69-5
Molecular Formula:C₁₈H₁₈N₄O₆
Molecular Weight:386.364
Hs Code.:

Synonyms:(R)-3-[4-(2-allyl-6-nitro-2,3-dihydro-imidazo[2,1-b]oxazol-2-yl)-phenyl]-5-hydroxymethyl-oxazolidin-2-one

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Chemical Property of (R)-3-[4-(2-allyl-6-nitro-2,3-dihydro-imidazo[2,1-b]oxazol-2-yl)-phenyl]-5-hydroxymethyl-oxazolidin-2-one

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Technology Process of (R)-3-[4-(2-allyl-6-nitro-2,3-dihydro-imidazo[2,1-b]oxazol-2-yl)-phenyl]-5-hydroxymethyl-oxazolidin-2-one

There total 3 articles about (R)-3-[4-(2-allyl-6-nitro-2,3-dihydro-imidazo[2,1-b]oxazol-2-yl)-phenyl]-5-hydroxymethyl-oxazolidin-2-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1188337-70-3
butyric acid (R)-3-[4-(2-allyl-6-nitro-2,3-dihydro-imidazo[2,1-b]oxazol-2-yl)-phenyl]-2-oxo-oxazolidin-5-ylmethyl ester

: 1188918-69-5
(R)-3-[4-(2-allyl-6-nitro-2,3-dihydro-imidazo[2,1-b]oxazol-2-yl)-phenyl]-5-hydroxymethyl-oxazolidin-2-one

Guidance literature:: butyric acid (R)-3-[4-(2-allyl-6-nitro-2,3-dihydro-imidazo[2,1-b]oxazol-2-yl)-phenyl]-2-oxo-oxazolidin-5-ylmethyl ester; With methanol; potassium carbonate; In dichloromethane; at 20 ℃; for 1.5h;

With acetic acid; In methanol; dichloromethane; water;

Reference yield:

: 1188337-68-9
butyric acid (R)-3-{4-[2-(2-chloro-4-nitro-imidazol-1-yl)-acetyl]-phenyl}-2-oxo-oxazolidin-5-ylmethyl ester

: 1188918-69-5
(R)-3-[4-(2-allyl-6-nitro-2,3-dihydro-imidazo[2,1-b]oxazol-2-yl)-phenyl]-5-hydroxymethyl-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: indium / N,N-dimethyl-formamide / 1 h / 50 °C

1.2: 3.5 h / 50 °C

2.1: caesium carbonate / N,N-dimethyl-formamide / 18 h / 50 °C

3.1: methanol; potassium carbonate / dichloromethane / 1.5 h / 20 °C

With methanol; indium; potassium carbonate; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide;

Reference yield:

: 128781-71-5
(R)-<3-<4-(bromoacetyl)phenyl>-2-oxo-5-oxazolidinyl>methyl butyrate

: 1188918-69-5
(R)-3-[4-(2-allyl-6-nitro-2,3-dihydro-imidazo[2,1-b]oxazol-2-yl)-phenyl]-5-hydroxymethyl-oxazolidin-2-one

Guidance literature:: Multi-step reaction with 4 steps

1.1: potassium carbonate / acetonitrile / 2 h / 60 °C

2.1: indium / N,N-dimethyl-formamide / 1 h / 50 °C

2.2: 3.5 h / 50 °C

3.1: caesium carbonate / N,N-dimethyl-formamide / 18 h / 50 °C

4.1: methanol; potassium carbonate / dichloromethane / 1.5 h / 20 °C

With methanol; indium; potassium carbonate; caesium carbonate; In dichloromethane; N,N-dimethyl-formamide; acetonitrile;