diphenyl ((3,5-di-tert-butyl-4-oxocyclohexa-2,5-dien-1-ylidene)methyl)phosphonate

Base Information

• Chemical Name: diphenyl ((3,5-di-tert-butyl-4-oxocyclohexa-2,5-dien-1-ylidene)methyl)phosphonate
• CAS No.: 1385088-92-5
• Molecular Formula: C₂₇H₃₁O₄P
• Molecular Weight: 450.514

Synonyms:diphenyl ((3,5-di-tert-butyl-4-oxocyclohexa-2,5-dien-1-ylidene)methyl)phosphonate

Chemical Property of diphenyl ((3,5-di-tert-butyl-4-oxocyclohexa-2,5-dien-1-ylidene)methyl)phosphonate

Chemical Property:

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Technology Process of diphenyl ((3,5-di-tert-butyl-4-oxocyclohexa-2,5-dien-1-ylidene)methyl)phosphonate

There total 1 articles about diphenyl ((3,5-di-tert-butyl-4-oxocyclohexa-2,5-dien-1-ylidene)methyl)phosphonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

diphenyl (3,5-di-tert-butyl-4-hydroxybenzyl)phosphonate (6731-96-0) → diphenyl ((3,5-di-tert-butyl-4-oxocyclohexa-2,5-dien-1-ylidene)methyl)phosphonate (1385088-92-5)

Guidance literature:

With potassium hydroxide; potassium hexacyanoferrate(III); In benzene; at 20 ℃; for 3h;

DOI:10.1007/s11172-011-0303-8

Reference yield: 98.0%

diphenyl ((3,5-di-tert-butyl-4-oxocyclohexa-2,5-dien-1-ylidene)methyl)phosphonate (1385088-92-5) + m-phenylenediamine (108-45-2,64554-26-3,76583-20-5) → diphenyl [(3,5-di-tert-butyl-4-hydroxyphenyl)(2,4-diaminophenyl)methyl]phosphonate

Guidance literature:

In 1,4-dioxane; at 20 ℃; for 6h;

DOI:10.1007/s11172-014-0619-2

Reference yield: 98.0%

SEC-BUTYLAMINE (33966-50-6) + diphenyl ((3,5-di-tert-butyl-4-oxocyclohexa-2,5-dien-1-ylidene)methyl)phosphonate (1385088-92-5) → diphenyl [(sec-butylamino)(3,5-di-tert-butyl-4-hydroxyphenyl)methyl]phosphonate (1594963-57-1)

Guidance literature:

In 1,4-dioxane; at 20 ℃; for 1h;

DOI:10.1007/s11172-013-0233-8

upstream raw materials:

diphenyl (3,5-di-tert-butyl-4-hydroxybenzyl)phosphonate

Downstream raw materials:

diphenyl (3,5-di-tert-butyl-4-hydroxyphenyl)(4-hydroxyphenyl)methylphosphonate

diphenyl [(n-butylamino)(3,5-di-tert-butyl-4-hydroxyphenyl)methyl]phosphonate

diphenyl [(sec-butylamino)(3,5-di-tert-butyl-4-hydroxyphenyl)methyl]phosphonate

diphenyl [(3,5-di-tert-butyl-4-hydroxyphenyl)(dodecylamino)methyl]phosphonate

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