1-(allyloxy)-4-benzylbenzene

Base Information

Chemical Name:1-(allyloxy)-4-benzylbenzene
CAS No.:131866-07-4
Molecular Formula:C₁₆H₁₆O
Molecular Weight:224.302
Hs Code.:

Synonyms:1-(allyloxy)-4-benzylbenzene

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Chemical Property of 1-(allyloxy)-4-benzylbenzene

Chemical Property:

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Technology Process of 1-(allyloxy)-4-benzylbenzene

There total 2 articles about 1-(allyloxy)-4-benzylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 100-44-7
benzyl chloride

: 4-(2-propen-1-yloxy)phenyl boronic acid

: 131866-07-4
1-(allyloxy)-4-benzylbenzene

Guidance literature:: With 1-methyl-2-azepanone; copper(l) iodide; 2,2,6,6-tetramethylheptane-3,5-dione; lithium tert-butoxide; at 60 ℃; for 12h; Schlenk technique; Inert atmosphere;
DOI:10.1039/c4cc05376a

Reference yield:

: 101-53-1
p-benzylphenol

: 106-95-6
allyl bromide

: 131866-07-4
1-(allyloxy)-4-benzylbenzene

Guidance literature:: With potassium hydroxide;

Reference yield:

: 124-38-9,18923-20-1
carbon dioxide

: 131866-07-4
1-(allyloxy)-4-benzylbenzene

: C₁₇H₁₆O₃

Guidance literature:: 1-(allyloxy)-4-benzylbenzene; With 2,2,6,6-tetramethylpiperidinyl-lithium; triisobutylaluminum; In tetrahydrofuran; hexane; at -78 - 20 ℃; for 3h; Inert atmosphere;

carbon dioxide; With [(1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidene)Cu(O-tBu)]; In tetrahydrofuran; at -78 - 0 ℃; for 2h; under 760.051 Torr; Inert atmosphere;

With hydrogenchloride; In water; at 0 ℃; Inert atmosphere;
DOI:10.1039/c7ob00341b