C₂₀H₂₆INO₄

Base Information

Chemical Name:C₂₀H₂₆INO₄
CAS No.:1267652-02-7
Molecular Formula:C₂₀H₂₆INO₄
Molecular Weight:471.335
Hs Code.:

C<sub>20</sub>H<sub>26</sub>INO<sub>4</sub>

Synonyms:C₂₀H₂₆INO₄

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Chemical Property of C₂₀H₂₆INO₄

Chemical Property:

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Technology Process of C₂₀H₂₆INO₄

There total 23 articles about C₂₀H₂₆INO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 1267652-00-5
C₃₂H₅₃NO₄Sn

: 1267652-02-7
C₂₀H₂₆INO₄

Guidance literature:: With iodine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol103094j

Reference yield:

: 1267651-99-9
C₂₀H₂₅NO₄

: 1267652-02-7
C₂₀H₂₆INO₄

Guidance literature:: C₂₀H₂₅NO₄; With bis-triphenylphosphine-palladium(II) chloride; tri-n-butyl-tin hydride; In tetrahydrofuran; at 20 ℃; for 0.5h; Inert atmosphere;

With iodine; In dichloromethane; at 0 - 20 ℃; Inert atmosphere;
DOI:10.1021/ol103094j

Reference yield:

: 870137-18-1
(R)-4-((R)-1-hydroxy-1-methylprop-2-ynyl)-2,2-dimethyl-oxazolidine-3-carboxylic acid tert-butyl ester

: 1267652-02-7
C₂₀H₂₆INO₄

Guidance literature:: Multi-step reaction with 19 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 4 h / 20 °C / Inert atmosphere

2.1: 1,4-bis-(9-O-dihydroquinidinyl)phthalazine; methanesulfonamide / water; tert-butyl alcohol / 24 h / 20 °C

3.1: dmap; triethylamine / dichloromethane / 3 h / 20 °C / Inert atmosphere

4.1: tetra-(n-butyl)ammonium iodide; N-ethyl-N,N-diisopropylamine / 1,2-dichloro-ethane / 12 h / 50 °C / Inert atmosphere

5.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

6.1: toluene-4-sulfonic acid / methanol / 2 h / 20 °C

7.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

8.1: tetrahydrofuran / 0 - 20 °C / Inert atmosphere

9.1: sodium hexamethyldisilazane / tetrahydrofuran / 0.25 h / 0 °C / Inert atmosphere

9.2: 0 - 20 °C / Inert atmosphere

10.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

11.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / dichloromethane / 2 h / 50 °C / Inert atmosphere

12.1: propan-1-ol; potassium hydroxide / water / 12 h / Reflux

13.1: sodium carbonate / tetrahydrofuran; water / 3 h / 0 °C

14.1: oxone; Na₂EDTA; 1,1,1-trifluoro-2-propanone; sodium hydrogencarbonate / water; acetonitrile / 3 h / 0 °C

15.1: Dess-Martin periodane / dichloromethane / 20 °C

16.1: tetrahydrofuran / -78 - 0 °C / Inert atmosphere

17.1: triethylamine / dichloromethane / 1 h / 0 - 20 °C / Inert atmosphere

18.1: piperidine / acetonitrile / 12 h / 20 °C / Inert atmosphere

19.1: bis-triphenylphosphine-palladium(II) chloride; tri-n-butyl-tin hydride / tetrahydrofuran / 0.5 h / 20 °C / Inert atmosphere

19.2: 0 - 20 °C / Inert atmosphere

With piperidine; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; propan-1-ol; dmap; bis-triphenylphosphine-palladium(II) chloride; 1,4-bis-(9-O-dihydroquinidinyl)phthalazine; oxone; lithium aluminium tetrahydride; methanesulfonamide; 1,1,1-trifluoro-2-propanone; Na₂EDTA; tetrabutyl ammonium fluoride; tri-n-butyl-tin hydride; sodium hexamethyldisilazane; tetra-(n-butyl)ammonium iodide; sodium hydrogencarbonate; sodium carbonate; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane; acetonitrile; tert-butyl alcohol; 16.1: Grignard reaction;
DOI:10.1021/ol103094j