2',4-bis(carboxymethoxy)-4'-(3-hydroxymethyl-2-butenyloxy)dihydrochalcone

Base Information

Chemical Name:2',4-bis(carboxymethoxy)-4'-(3-hydroxymethyl-2-butenyloxy)dihydrochalcone
CAS No.:98314-75-1
Molecular Formula:C₂₄H₂₆O₉
Molecular Weight:458.465
Hs Code.:

Synonyms:2',4-bis(carboxymethoxy)-4'-(3-hydroxymethyl-2-butenyloxy)dihydrochalcone

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Chemical Property of 2',4-bis(carboxymethoxy)-4'-(3-hydroxymethyl-2-butenyloxy)dihydrochalcone

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Technology Process of 2',4-bis(carboxymethoxy)-4'-(3-hydroxymethyl-2-butenyloxy)dihydrochalcone

There total 9 articles about 2',4-bis(carboxymethoxy)-4'-(3-hydroxymethyl-2-butenyloxy)dihydrochalcone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 98314-78-4
{5-((E)-4-Hydroxy-3-methyl-but-2-enyloxy)-2-[3-(4-methoxycarbonylmethoxy-phenyl)-propionyl]-phenoxy}-acetic acid methyl ester

: 98314-75-1
2',4-bis(carboxymethoxy)-4'-(3-hydroxymethyl-2-butenyloxy)dihydrochalcone

Guidance literature:: With potassium hydroxide; In methanol; water; for 1h;
DOI:10.1248/cpb.33.1327

Reference yield:

: 29682-12-0
1-[4-(benzyloxy)-2-hydroxyphenyl]ethanone

: 98314-75-1
2',4-bis(carboxymethoxy)-4'-(3-hydroxymethyl-2-butenyloxy)dihydrochalcone

Guidance literature:: Multi-step reaction with 7 steps

1: 91 percent / KOH / acetone / 8 h / Ambient temperature

2: 93 percent / H₂ / Pd-C (10percent) / methanol; dioxane

3: 85 percent / NaOH / H₂O; ethanol / 8 h / Ambient temperature

4: 76 percent / concd. HCl / 7 h / Heating

5: 63 percent / H₂ / Pd-C (10percent) / methanol; dioxane

6: 76 percent / K₂CO₃, KI / acetone / 10 h / Ambient temperature

7: 75 percent / KOH / H₂O; methanol / 1 h

With hydrogenchloride; potassium hydroxide; sodium hydroxide; hydrogen; potassium carbonate; potassium iodide; palladium on activated charcoal; In 1,4-dioxane; methanol; ethanol; water; acetone;
DOI:10.1248/cpb.33.1327

Reference yield:

: 89-84-9
2',4'-dihydroxy-4-acetophenone

: 98314-75-1
2',4-bis(carboxymethoxy)-4'-(3-hydroxymethyl-2-butenyloxy)dihydrochalcone

Guidance literature:: Multi-step reaction with 8 steps

1: 80 percent / K₂CO₃ / acetone / 4 h / 50 °C

2: 91 percent / KOH / acetone / 8 h / Ambient temperature

3: 93 percent / H₂ / Pd-C (10percent) / methanol; dioxane

4: 85 percent / NaOH / H₂O; ethanol / 8 h / Ambient temperature

5: 76 percent / concd. HCl / 7 h / Heating

6: 63 percent / H₂ / Pd-C (10percent) / methanol; dioxane

7: 76 percent / K₂CO₃, KI / acetone / 10 h / Ambient temperature

8: 75 percent / KOH / H₂O; methanol / 1 h

With hydrogenchloride; potassium hydroxide; sodium hydroxide; hydrogen; potassium carbonate; potassium iodide; palladium on activated charcoal; In 1,4-dioxane; methanol; ethanol; water; acetone;
DOI:10.1248/cpb.33.1327