Eu(II)[[(2,6-iPr₂C₆H₃)NC(Me)CHC(Me)N-(C₆H₅)](-)]2

Base Information

• Chemical Name: Eu(II)[[(2,6-iPr₂C₆H₃)NC(Me)CHC(Me)N-(C₆H₅)](-)]2
• CAS No.: 1362987-60-7
• Molecular Formula: C₄₆H₅₈EuN₄
• Molecular Weight: 818.953

Synonyms:Eu(II)[[(2,6-iPr₂C₆H₃)NC(Me)CHC(Me)N-(C₆H₅)](-)]2

Chemical Property of Eu(II)[[(2,6-iPr₂C₆H₃)NC(Me)CHC(Me)N-(C₆H₅)](-)]2

Chemical Property:

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Technology Process of Eu(II)[[(2,6-iPr₂C₆H₃)NC(Me)CHC(Me)N-(C₆H₅)](-)]2

There total 2 articles about Eu(II)[[(2,6-iPr₂C₆H₃)NC(Me)CHC(Me)N-(C₆H₅)](-)]2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

europioum(III) chloride + C23H29N2(1-)*Na(1+) → Eu(II)[[(2,6-iPr2C6H3)NC(Me)CHC(Me)N-(C6H5)](-)]2 (1362987-60-7)

Guidance literature:

europioum(III) chloride; C₂₃H₂₉N₂^(1-)*Na⁽¹⁺⁾; In tetrahydrofuran; at 20 ℃; Inert atmosphere; Schlenk technique;

With sodium-potassium alloy; In tetrahydrofuran; toluene; at 20 ℃; Inert atmosphere; Schlenk technique;

DOI:10.1039/c5dt03674g

Reference yield: 23.0%

[((C3H7)2C6H3)NC(CH3)CHC(CH3)N(C6H5)](1-)*Na(1+)=[((C3H7)2C6H3)NC(CH3)CHC(CH3)N(C6H5)]Na + europium(III) chloride (10025-76-0) → Eu(II)[[(2,6-iPr2C6H3)NC(Me)CHC(Me)N-(C6H5)](-)]2 (1362987-60-7)

Guidance literature:

In tetrahydrofuran; under Ar; to soln. of ligand was added slurry of EuCl3 in THF at room temp., mixt. was stirred at 60°C for 24 h; ppt. was removed by centrifugation, soln. was concd. to dryness, then THF and hexane were added, ppt. was crystd. at room temp.; elem. anal.;

DOI:10.1039/c2dt12176j

upstream raw materials:

europium(III) chloride

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