Technology Process of 1-(6-hydroxyhexyloxy)-5-(methoxymethyl)-2,3,4,6-tetramethylbenzene
There total 5 articles about 1-(6-hydroxyhexyloxy)-5-(methoxymethyl)-2,3,4,6-tetramethylbenzene which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
potassium carbonate;
potassium iodide;
In
acetonitrile;
for 72h;
Heating;
DOI:10.1021/ma0508146
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 57 percent / methanol / 13 h / Heating
2: 79 percent / K2CO3 / KI / acetonitrile / 72 h / Heating
With
potassium carbonate;
potassium iodide;
In
methanol; acetonitrile;
DOI:10.1021/ma0508146
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 92 percent / NaBr; acetic acid; H2SO4 / 1 h / 20 °C
2: 77 percent / LiAlH4 / diethyl ether / 0.5 h / 20 °C
3: NaBr; acetic acid; H2SO4 / 12 h / 20 °C
4: 57 percent / methanol / 13 h / Heating
5: 79 percent / K2CO3 / KI / acetonitrile / 72 h / Heating
With
lithium aluminium tetrahydride; sulfuric acid; potassium carbonate; acetic acid; sodium bromide;
potassium iodide;
In
methanol; diethyl ether; acetonitrile;
DOI:10.1021/ma0508146
