(1S)-2,3,4,6-tetra-O-acetyl-1-[2-(acetyloxy)-5-[(4-bromo-2-methylphenyl)methyl]-4-(propan-2-yl)phenyl]-1,5-anhydro-D-glucitol

Base Information

Chemical Name:(1S)-2,3,4,6-tetra-O-acetyl-1-[2-(acetyloxy)-5-[(4-bromo-2-methylphenyl)methyl]-4-(propan-2-yl)phenyl]-1,5-anhydro-D-glucitol
CAS No.:1240304-31-7
Molecular Formula:C₃₃H₃₉BrO₁₁
Molecular Weight:691.57
Hs Code.:

Synonyms:(1S)-2,3,4,6-tetra-O-acetyl-1-[2-(acetyloxy)-5-[(4-bromo-2-methylphenyl)methyl]-4-(propan-2-yl)phenyl]-1,5-anhydro-D-glucitol

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Chemical Property of (1S)-2,3,4,6-tetra-O-acetyl-1-[2-(acetyloxy)-5-[(4-bromo-2-methylphenyl)methyl]-4-(propan-2-yl)phenyl]-1,5-anhydro-D-glucitol

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Technology Process of (1S)-2,3,4,6-tetra-O-acetyl-1-[2-(acetyloxy)-5-[(4-bromo-2-methylphenyl)methyl]-4-(propan-2-yl)phenyl]-1,5-anhydro-D-glucitol

There total 26 articles about (1S)-2,3,4,6-tetra-O-acetyl-1-[2-(acetyloxy)-5-[(4-bromo-2-methylphenyl)methyl]-4-(propan-2-yl)phenyl]-1,5-anhydro-D-glucitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1240304-51-1
C₃₃H₃₉BrO₁₂

: 1240304-31-7
(1S)-2,3,4,6-tetra-O-acetyl-1-[2-(acetyloxy)-5-[(4-bromo-2-methylphenyl)methyl]-4-(propan-2-yl)phenyl]-1,5-anhydro-D-glucitol

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In chloroform; acetonitrile; at 4 - 20 ℃; for 0.5h; Inert atmosphere;

Reference yield:

: C₃₅H₄₁BrO₁₃

: 1240304-31-7
(1S)-2,3,4,6-tetra-O-acetyl-1-[2-(acetyloxy)-5-[(4-bromo-2-methylphenyl)methyl]-4-(propan-2-yl)phenyl]-1,5-anhydro-D-glucitol

Guidance literature:: With triethylsilane; boron trifluoride diethyl etherate; In chloroform; acetonitrile; at 4 ℃; for 0.666667h; Inert atmosphere;
DOI:10.1016/j.bmc.2018.12.015

Reference yield:

: 1359948-58-5
C₃₆H₄₃BrO₁₄

: 108-24-7
acetic anhydride

: 1240304-31-7
(1S)-2,3,4,6-tetra-O-acetyl-1-[2-(acetyloxy)-5-[(4-bromo-2-methylphenyl)methyl]-4-(propan-2-yl)phenyl]-1,5-anhydro-D-glucitol

Guidance literature:: C₃₆H₄₃BrO₁₄; With trimethylsilyl trifluoromethanesulfonate; tert-butyldimethylsilane; In water; acetonitrile; for 1.5h; Cooling;

acetic anhydride; In water; acetonitrile; for 0.416667h; Cooling;