p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-galactopyranoside

Base Information

• Chemical Name: p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-galactopyranoside
• CAS No.: 1206803-32-8
• Molecular Formula: C₄₀H₅₀O₇Si
• Molecular Weight: 670.918

Synonyms:p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-galactopyranoside

Chemical Property of p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-galactopyranoside

Chemical Property:

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Technology Process of p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-galactopyranoside

There total 1 articles about p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

triethylsilane (617-86-7) + p-methoxyphenyl 2,3,4,6-tetra-O-benzyl-β-D-galactopyranoside (143536-99-6) → p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-galactopyranoside (1206803-32-8)

Guidance literature:

triethylsilane; With dicobalt octacarbonyl; carbon monoxide; at 20 ℃; for 0.25h; under 760.051 Torr;

p-methoxyphenyl 2,3,4,6-tetra-O-benzyl-β-D-galactopyranoside; In benzene; at 50 ℃; for 30h; regioselective reaction;

DOI:10.1021/ol902717y

Reference yield:

p-methoxyphenyl 2,3,4-tri-O-benzyl-6-O-triethyl-silyl-β-D-galactopyranoside (1206803-32-8) → 4-methoxyphenyl 2,3,4-tri-O-benzyl-β-D-galactopyranoside (129163-33-3)

Guidance literature:

With tetrabutyl ammonium fluoride; water; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1021/ol902717y

upstream raw materials:

triethylsilane

p-methoxyphenyl 2,3,4,6-tetra-O-benzyl-β-D-galactopyranoside

Downstream raw materials:

4-methoxyphenyl 2,3,4-tri-O-benzyl-β-D-galactopyranoside

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