Technology Process of 3-pentylphenylboronic acid
There total 5 articles about 3-pentylphenylboronic acid which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: potassium hydrogen fluoride / methanol; water / 0.5 h
2: chloro-trimethyl-silane; water / acetonitrile / 1 h
With
chloro-trimethyl-silane; potassium hydrogen fluoride; water;
In
methanol; water; acetonitrile;
DOI:10.1016/j.bmcl.2011.12.043
- Guidance literature:
-
Multi-step reaction with 6 steps
1: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; potassium phosphate monohydrate; palladium diacetate / toluene
2: palladium on activated charcoal; hydrogen / ethanol
3: hydrogenchloride; sodium nitrite / water / Cooling with ice
4: dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; palladium diacetate; triethylamine / 1,4-dioxane / 80 °C
5: potassium hydrogen fluoride / methanol; water / 0.5 h
6: chloro-trimethyl-silane; water / acetonitrile / 1 h
With
dicyclohexyl-(2',6'-dimethoxybiphenyl-2-yl)-phosphane; hydrogenchloride; chloro-trimethyl-silane; potassium phosphate monohydrate; potassium hydrogen fluoride; palladium on activated charcoal; water; hydrogen; palladium diacetate; triethylamine; sodium nitrite;
In
1,4-dioxane; methanol; ethanol; water; toluene; acetonitrile;
1: Suzuki coupling;
DOI:10.1016/j.bmcl.2011.12.043
