C₄₂H₄₁OPS

Base Information

Chemical Name:C₄₂H₄₁OPS
CAS No.:1293287-07-6
Molecular Formula:C₄₂H₄₁OPS
Molecular Weight:624.827
Hs Code.:

Synonyms:C₄₂H₄₁OPS

Suppliers and Price of C₄₂H₄₁OPS

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Chemical Property of C₄₂H₄₁OPS

Chemical Property:

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Technology Process of C₄₂H₄₁OPS

There total 4 articles about C₄₂H₄₁OPS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 1293287-12-3
diphenyl(4-ethynylphenyl)phosphane sulfide

: 1293287-08-7
[(E)-1-iodo-4-(4-octyloxy)styryl]benzene

: 1293287-07-6
C₄₂H₄₁OPS

Guidance literature:: With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; diisopropylamine; In toluene; at 50 ℃; for 15h;
DOI:10.1002/asia.201000681

Reference yield:

: 15164-44-0
p-(iodophenyl)carboxaldehyde

: 1293287-07-6
C₄₂H₄₁OPS

Guidance literature:: Multi-step reaction with 2 steps

1.1: 18-crown-6 ether; sodium hydride / tetrahydrofuran / 20 °C

1.2: 20 °C / Irradiation

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diisopropylamine / toluene / 15 h / 50 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 18-crown-6 ether; sodium hydride; diisopropylamine; In tetrahydrofuran; toluene; 1.1: Wittig reaction / 2.1: Sonogashira coupling;
DOI:10.1002/asia.201000681

Reference yield:

: p-n-octyloxybenzyl triphenylphosphonium bromide

: 1293287-07-6
C₄₂H₄₁OPS

Guidance literature:: Multi-step reaction with 2 steps

1.1: 18-crown-6 ether; sodium hydride / tetrahydrofuran / 20 °C

1.2: 20 °C / Irradiation

2.1: copper(l) iodide; bis-triphenylphosphine-palladium(II) chloride; diisopropylamine / toluene / 15 h / 50 °C

With bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; 18-crown-6 ether; sodium hydride; diisopropylamine; In tetrahydrofuran; toluene; 1.1: Wittig reaction / 2.1: Sonogashira coupling;
DOI:10.1002/asia.201000681