ANTHRAQUINONE MONOHYDRAZONE

Base Information

• Chemical Name: ANTHRAQUINONE MONOHYDRAZONE
• CAS No.: 3166-13-0
• Molecular Formula: C14H10 N2 O
• Molecular Weight: 222.246
• Hs Code.: 2928000090
• Mol file: 3166-13-0.mol

Synonyms:9,10-Anthracenedione,monohydrazone (9CI); Anthraquinone, hydrazone (7CI); Anthraquinone,monohydrazone (8CI)

Chemical Property of ANTHRAQUINONE MONOHYDRAZONE

Chemical Property:

• Vapor Pressure: 6.72E-07mmHg at 25°C
• Boiling Point: 409°C at 760 mmHg
• PKA: -0.63±0.20(Predicted)
• Flash Point: 201.1°C
• PSA: 55.45000
• Density: 1.29g/cm³
• LogP: 2.64240

Purity/Quality:

98%Min ^*data from raw suppliers

ANTHRAQUINONE MONOHYDRAZONE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of ANTHRAQUINONE MONOHYDRAZONE

There total 5 articles about ANTHRAQUINONE MONOHYDRAZONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 20.0%

anthracen-9(10H)-one (90-44-8) → 10-hydrazono-9,10-dihydroanthracen-9-one (3166-13-0) + 9,10-phenanthrenequinone (84-65-1)

Guidance literature:

With sulfur; hydrazine hydrate; In N,N-dimethyl-formamide; at 20 - 25 ℃; for 5h;

Reference yield:

Anthrachinon-(9,10)-triphenylphosphazin (1705-80-2) → 10-hydrazono-9,10-dihydroanthracen-9-one (3166-13-0)

Guidance literature:

With acetic acid; In ethanol;

Reference yield:

10-diazo-10H-anthracen-9-one (1705-82-4) → 10-hydrazono-9,10-dihydroanthracen-9-one (3166-13-0)

Guidance literature:

Multi-step reaction with 2 steps

1: acetonitrile

2: AcOH / aq. ethanol

With acetic acid; In ethanol; acetonitrile;

upstream raw materials:

Anthrachinon-(9,10)-triphenylphosphazin

anthracen-9(10H)-one

10-diazo-10H-anthracen-9-one

Downstream raw materials:

9-benzylidenehydrazono-10-anthrone

Refernces