1-(tert-butyldiphenylsilyloxymethyl)-1-(2-hydroxyethyl)-2,5-cyclohexadiene

Base Information

Chemical Name:1-(tert-butyldiphenylsilyloxymethyl)-1-(2-hydroxyethyl)-2,5-cyclohexadiene
CAS No.:868979-50-4
Molecular Formula:C₂₅H₃₂O₂Si
Molecular Weight:392.613
Hs Code.:

Synonyms:1-(tert-butyldiphenylsilyloxymethyl)-1-(2-hydroxyethyl)-2,5-cyclohexadiene

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(tert-butyldiphenylsilyloxymethyl)-1-(2-hydroxyethyl)-2,5-cyclohexadiene

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Technology Process of 1-(tert-butyldiphenylsilyloxymethyl)-1-(2-hydroxyethyl)-2,5-cyclohexadiene

There total 4 articles about 1-(tert-butyldiphenylsilyloxymethyl)-1-(2-hydroxyethyl)-2,5-cyclohexadiene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1-[2-(tert-butyl-dimethyl-silanyloxy)-ethyl]-cyclohexa-2,5-dienecarboxylic acid methyl ester

: 868979-50-4
1-(tert-butyldiphenylsilyloxymethyl)-1-(2-hydroxyethyl)-2,5-cyclohexadiene

Guidance literature:: Multi-step reaction with 3 steps

1: 8.4 g / DIBAL-H / tetrahydrofuran; hexane / 1 h / -78 °C

2: i-Pr₂NEt / 0 - 20 °C

3: 1.7 g / aq. AcOH / 2 h / Heating

With diisobutylaluminium hydride; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane;
DOI:10.1248/cpb.53.952

Reference yield:

: 30889-20-4
methyl cyclohexa-2,5-diene-1-carboxylate

: 868979-50-4
1-(tert-butyldiphenylsilyloxymethyl)-1-(2-hydroxyethyl)-2,5-cyclohexadiene

Guidance literature:: Multi-step reaction with 4 steps

1: tetrahydrofuran / 0.33 h / -78 °C

2: 8.4 g / DIBAL-H / tetrahydrofuran; hexane / 1 h / -78 °C

3: i-Pr₂NEt / 0 - 20 °C

4: 1.7 g / aq. AcOH / 2 h / Heating

With diisobutylaluminium hydride; acetic acid; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; hexane;
DOI:10.1248/cpb.53.952