5-(tert-butyl)-4-phenyl-6-(phenylsulfanyl)-2,3-benzo-1,3a,6a-triazapentalene

Base Information

Chemical Name:5-(tert-butyl)-4-phenyl-6-(phenylsulfanyl)-2,3-benzo-1,3a,6a-triazapentalene
CAS No.:433295-89-7
Molecular Formula:C₂₅H₂₃N₃S
Molecular Weight:397.544
Hs Code.:

Synonyms:5-(tert-butyl)-4-phenyl-6-(phenylsulfanyl)-2,3-benzo-1,3a,6a-triazapentalene

Suppliers and Price of 5-(tert-butyl)-4-phenyl-6-(phenylsulfanyl)-2,3-benzo-1,3a,6a-triazapentalene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 5-(tert-butyl)-4-phenyl-6-(phenylsulfanyl)-2,3-benzo-1,3a,6a-triazapentalene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 5-(tert-butyl)-4-phenyl-6-(phenylsulfanyl)-2,3-benzo-1,3a,6a-triazapentalene

There total 5 articles about 5-(tert-butyl)-4-phenyl-6-(phenylsulfanyl)-2,3-benzo-1,3a,6a-triazapentalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 1-(2-benzenesulfinylmethyl-3,3-dimethyl-1-phenylbut-1-enyl)-1H-benzotriazole

: 433295-89-7
5-(tert-butyl)-4-phenyl-6-(phenylsulfanyl)-2,3-benzo-1,3a,6a-triazapentalene

Guidance literature:: With trifluoroacetic anhydride; In tetrahydrofuran; at 25 ℃; for 1h;
DOI:10.1002/1099-0690(20022)2002:3<493::AID-EJOC493>3.0.CO;2-B

Reference yield:

: 108-98-5
thiophenol

: 433295-89-7
5-(tert-butyl)-4-phenyl-6-(phenylsulfanyl)-2,3-benzo-1,3a,6a-triazapentalene

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium / ethanol / 0.08 h

1.2: 70 percent / ethanol; tetrahydrofuran / 5 h / 20 °C

2.1: 86 percent / mCPBA / CH₂Cl₂ / 0.08 h / 25 °C

3.1: 88 percent / trifluoroacetic anhydride / tetrahydrofuran / 1 h / 25 °C

With sodium; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1002/1099-0690(20022)2002:3<493::AID-EJOC493>3.0.CO;2-B

Reference yield:

: 627088-05-5
3-(benzotriazol-1-yl)-2-(tert-butyl)-3-phenyl-2-propenol

: 433295-89-7
5-(tert-butyl)-4-phenyl-6-(phenylsulfanyl)-2,3-benzo-1,3a,6a-triazapentalene

Guidance literature:: Multi-step reaction with 4 steps

1.1: 87 percent / SOCl₂ / tetrahydrofuran / 1 h / 25 °C

2.1: sodium / ethanol / 0.08 h

2.2: 70 percent / ethanol; tetrahydrofuran / 5 h / 20 °C

3.1: 86 percent / mCPBA / CH₂Cl₂ / 0.08 h / 25 °C

4.1: 88 percent / trifluoroacetic anhydride / tetrahydrofuran / 1 h / 25 °C

With thionyl chloride; sodium; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic anhydride; In tetrahydrofuran; ethanol; dichloromethane;
DOI:10.1002/1099-0690(20022)2002:3<493::AID-EJOC493>3.0.CO;2-B