cirsiliol 5-hexyl ether

Base Information

Chemical Name:cirsiliol 5-hexyl ether
CAS No.:103776-69-8
Molecular Formula:C₂₃H₂₆O₇
Molecular Weight:414.455
Hs Code.:

Synonyms:cirsiliol 5-hexyl ether

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Chemical Property of cirsiliol 5-hexyl ether

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Technology Process of cirsiliol 5-hexyl ether

There total 8 articles about cirsiliol 5-hexyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 103777-21-5
2-(3,4-Bis-benzyloxy-phenyl)-5-hexyloxy-6,7-dimethoxy-chromen-4-one

: 103776-69-8
cirsiliol 5-hexyl ether

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; ethyl acetate;
DOI:10.1021/jm00161a021

Reference yield:

: 51145-78-9
2-(3,4-bis-benzyloxy-phenyl)-5,6,7-trimethoxy-chromen-4-one

: 103776-69-8
cirsiliol 5-hexyl ether

Guidance literature:: Multi-step reaction with 3 steps

1: 87 percent / AlCl₃ / acetonitrile / 1.5 h / 50 °C

2: 90 percent / K₂CO₃ / acetone; dimethylformamide / 8 h / Heating

3: 81 percent / H₂ / 10percent Pd/C / methanol; ethyl acetate

With aluminium trichloride; hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; ethyl acetate; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/jm00161a021

Reference yield:

: 55274-37-8
3'4'-dibenzyloxy-2-hydroxy-4,5,6-trimethoxydibenzoyl methane

: 103776-69-8
cirsiliol 5-hexyl ether

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / AcONa, AcOH / 3 h / 140 - 145 °C

2: 87 percent / AlCl₃ / acetonitrile / 1.5 h / 50 °C

3: 90 percent / K₂CO₃ / acetone; dimethylformamide / 8 h / Heating

4: 81 percent / H₂ / 10percent Pd/C / methanol; ethyl acetate

With aluminium trichloride; hydrogen; sodium acetate; potassium carbonate; acetic acid; palladium on activated charcoal; In methanol; ethyl acetate; N,N-dimethyl-formamide; acetone; acetonitrile;
DOI:10.1021/jm00161a021