2,3,4-tri-O-benzyl-5-deoxy-5-(9-fluorenyl-methyloxycarbonylamino)-β-D-arabinose

Base Information

Chemical Name:2,3,4-tri-O-benzyl-5-deoxy-5-(9-fluorenyl-methyloxycarbonylamino)-β-D-arabinose
CAS No.:263243-27-2
Molecular Formula:C₄₁H₃₉NO₆
Molecular Weight:641.764
Hs Code.:

Synonyms:2,3,4-tri-O-benzyl-5-deoxy-5-(9-fluorenyl-methyloxycarbonylamino)-β-D-arabinose

Suppliers and Price of 2,3,4-tri-O-benzyl-5-deoxy-5-(9-fluorenyl-methyloxycarbonylamino)-β-D-arabinose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 2,3,4-tri-O-benzyl-5-deoxy-5-(9-fluorenyl-methyloxycarbonylamino)-β-D-arabinose

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 2,3,4-tri-O-benzyl-5-deoxy-5-(9-fluorenyl-methyloxycarbonylamino)-β-D-arabinose

There total 1 articles about 2,3,4-tri-O-benzyl-5-deoxy-5-(9-fluorenyl-methyloxycarbonylamino)-β-D-arabinose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 161418-70-8
2,3,4-tri-O-benzyl-5-deoxy-5-(9-fluorenyl-methyloxycarbonylamino)-D-arabinitol

: 263243-27-2
2,3,4-tri-O-benzyl-5-deoxy-5-(9-fluorenyl-methyloxycarbonylamino)-β-D-arabinose

Guidance literature:: With oxalyl dichloride; dimethyl sulfoxide; triethylamine; In dichloromethane; at -78 ℃; for 0.666667h;
DOI:10.1016/S0008-6215(99)00253-0

Reference yield:

: 263243-27-2
2,3,4-tri-O-benzyl-5-deoxy-5-(9-fluorenyl-methyloxycarbonylamino)-β-D-arabinose

: ethyl 2,3,4-tri-O-benzyl-5-deoxy-5-(9-fluorenylmethyloxycarbonylamino)-1-thio-D-arabinopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: 79 percent / 4 Angstroem molecular sieves; Me₃SiOTf / CH₂Cl₂ / 1.08 h / 0 °C

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In pyridine; dichloromethane; 1: Acetylation / 2: Substitution;
DOI:10.1016/S0008-6215(99)00253-0

Reference yield:

: 263243-27-2
2,3,4-tri-O-benzyl-5-deoxy-5-(9-fluorenyl-methyloxycarbonylamino)-β-D-arabinose

: cyclohexyl 2,3,4-tri-O-benzyl-5-deoxy-5-(9-fluorenylmethyloxycarbonylamino)-1-thio-D-arabinopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine

2: 73 percent / 4 Angstroem molecular sieves; Me₃SiOTf / CH₂Cl₂ / 1.08 h / 0 °C

With trimethylsilyl trifluoromethanesulfonate; 4 A molecular sieve; In pyridine; dichloromethane; 1: Acetylation / 2: Substitution;
DOI:10.1016/S0008-6215(99)00253-0