(+/-)N-benzyl-11-methoxynoraporphine

Base Information

Chemical Name:(+/-)N-benzyl-11-methoxynoraporphine
CAS No.:53581-08-1
Molecular Formula:C₂₄H₂₃NO
Molecular Weight:341.453
Hs Code.:

Synonyms:(+/-)N-benzyl-11-methoxynoraporphine

Suppliers and Price of (+/-)N-benzyl-11-methoxynoraporphine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)N-benzyl-11-methoxynoraporphine

Chemical Property:

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Technology Process of (+/-)N-benzyl-11-methoxynoraporphine

There total 3 articles about (+/-)N-benzyl-11-methoxynoraporphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 6-Benzyl-11-methoxy-5,6-dihydro-4H-dibenzo[de,g]quinoline

: 53581-08-1
(+/-)N-benzyl-11-methoxynoraporphine

Guidance literature:: With sulfuric acid; zinc; In ethanol; at 75 ℃; for 71h;
DOI:10.1021/jm960189i

Reference yield:

: 179952-75-1
Trifluoro-methanesulfonic acid (R)-6-benzyl-11-methoxy-5,6,6a,7-tetrahydro-4H-dibenzo[de,g]quinolin-10-yl ester

: 53581-08-1
(+/-)N-benzyl-11-methoxynoraporphine

Guidance literature:: Multi-step reaction with 2 steps

1: 3.8 percent / Bu₃N, HCO₂H, PPh₂(CH₂)3PPh₂, (PPh₃)2PdCl₂ / dimethylformamide / 18 h / 80 °C

2: Zn, 1M aq. H₂SO₄ / ethanol / 71 h / 75 °C

With bis-triphenylphosphine-palladium(II) chloride; formic acid; tributyl-amine; sulfuric acid; 1,3-bis-(diphenylphosphino)propane; zinc; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm960189i