1,4-bis<5-<2-<(5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl>-5-formyl-4-methylpyrrol-3-yl>pentyl>-2,3,5,6-tetramethylbenzene

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Chemical Name:1,4-bis<5-<2-<(5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl>-5-formyl-4-methylpyrrol-3-yl>pentyl>-2,3,5,6-tetramethylbenzene
CAS No.:102393-38-4
Molecular Formula:C₅₀H₆₆N₄O₆
Molecular Weight:819.097
Hs Code.:

Synonyms:1,4-bis<5-<2-<(5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl>-5-formyl-4-methylpyrrol-3-yl>pentyl>-2,3,5,6-tetramethylbenzene

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Chemical Property of 1,4-bis<5-<2-<(5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl>-5-formyl-4-methylpyrrol-3-yl>pentyl>-2,3,5,6-tetramethylbenzene

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Technology Process of 1,4-bis<5-<2-<(5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl>-5-formyl-4-methylpyrrol-3-yl>pentyl>-2,3,5,6-tetramethylbenzene

There total 23 articles about 1,4-bis<5-<2-<(5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl>-5-formyl-4-methylpyrrol-3-yl>pentyl>-2,3,5,6-tetramethylbenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 102393-35-1
1,4-bis<5-<2-<(5-ethoxycarbonyl-3-ethyl-4-methylpyrrol-2-yl)methyl>-5-(2,2-dicyanovinyl)-4-methylpyrrol-3-yl>pentyl>-2,3,5,6-tetramethylbenzene

: 102393-38-4
1,4-bis<5-<2-<(5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl>-5-formyl-4-methylpyrrol-3-yl>pentyl>-2,3,5,6-tetramethylbenzene

Guidance literature:: With potassium hydroxide; water; In propan-1-ol; Heating;

Reference yield:

: 2199-44-2
3,5-dimethyl-2-ethoxycarbonyl-1H-pyrrole

: 102393-38-4
1,4-bis<5-<2-<(5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl>-5-formyl-4-methylpyrrol-3-yl>pentyl>-2,3,5,6-tetramethylbenzene

Guidance literature:: Multi-step reaction with 11 steps

1: SnCl₂ / CH₂Cl₂; nitromethane / 1 h / Ambient temperature

2: 88.3 percent / B₂H₆ / tetrahydrofuran

3: 98.1 percent / PhCH₂ONa / Heating

4: H₂, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature

5: dimethylformamide / Heating

6: POCl₃ / CH₂Cl₂ / 0.5 h

7: NaHCO₃ / H₂O / Heating

8: cyclohexylamine / toluene / 2 h / Heating

9: SO₂Cl₂ / CH₂Cl₂ / Ambient temperature

10: glacial acetic acid / 1 h / 80 °C

11: 99 percent / H₂O, KOH / propan-1-ol / Heating

With potassium hydroxide; sulfuryl dichloride; water; hydrogen; sodium hydrogencarbonate; cyclohexylamine; acetic acid; triethylamine; sodium phenyl-methanolate; tin(ll) chloride; diborane; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; propan-1-ol; nitromethane; dichloromethane; water; N,N-dimethyl-formamide; toluene;

Reference yield:

: 2004-70-8,17410-45-6,25212-15-1,64940-84-7
1-methylbuta-1,3-diene

: 102393-38-4
1,4-bis<5-<2-<(5-carboxy-3-ethyl-4-methylpyrrol-2-yl)methyl>-5-formyl-4-methylpyrrol-3-yl>pentyl>-2,3,5,6-tetramethylbenzene

Guidance literature:: Multi-step reaction with 12 steps

1: Zn, acetic acid

2: SnCl₂ / CH₂Cl₂; nitromethane / 1 h / Ambient temperature

3: 88.3 percent / B₂H₆ / tetrahydrofuran

4: 98.1 percent / PhCH₂ONa / Heating

5: H₂, triethylamine / 10 percent Pd/C / tetrahydrofuran / Ambient temperature

6: dimethylformamide / Heating

7: POCl₃ / CH₂Cl₂ / 0.5 h

8: NaHCO₃ / H₂O / Heating

9: cyclohexylamine / toluene / 2 h / Heating

10: SO₂Cl₂ / CH₂Cl₂ / Ambient temperature

11: glacial acetic acid / 1 h / 80 °C

12: 99 percent / H₂O, KOH / propan-1-ol / Heating

With potassium hydroxide; sulfuryl dichloride; water; hydrogen; sodium hydrogencarbonate; cyclohexylamine; acetic acid; triethylamine; sodium phenyl-methanolate; tin(ll) chloride; diborane; zinc; trichlorophosphate; palladium on activated charcoal; In tetrahydrofuran; propan-1-ol; nitromethane; dichloromethane; water; N,N-dimethyl-formamide; toluene;