3-(4-chloro-trans-styryl)-4,6-dimethyl-6H-isoxazolo[3,4-d]pyridazin-7-one

Base Information

• Chemical Name: 3-(4-chloro-trans-styryl)-4,6-dimethyl-6H-isoxazolo[3,4-d]pyridazin-7-one
• CAS No.: 59761-65-8
• Molecular Formula: C₁₅H₁₂ClN₃O₂
• Molecular Weight: 301.732

Synonyms:3-(4-chloro-trans-styryl)-4,6-dimethyl-6H-isoxazolo[3,4-d]pyridazin-7-one

Chemical Property of 3-(4-chloro-trans-styryl)-4,6-dimethyl-6H-isoxazolo[3,4-d]pyridazin-7-one

Chemical Property:

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Technology Process of 3-(4-chloro-trans-styryl)-4,6-dimethyl-6H-isoxazolo[3,4-d]pyridazin-7-one

There total 4 articles about 3-(4-chloro-trans-styryl)-4,6-dimethyl-6H-isoxazolo[3,4-d]pyridazin-7-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

3-[2-(4-Chloro-phenyl)-2-hydroxy-ethyl]-4,6-dimethyl-6H-isoxazolo[3,4-d]pyridazin-7-one (109610-20-0) → 3-(4-chloro-trans-styryl)-4,6-dimethyl-6H-isoxazolo[3,4-d]pyridazin-7-one (59761-65-8)

Guidance literature:

With sulfuric acid; for 1h; Ambient temperature;

DOI:10.3987/R-1986-12-3467

Reference yield:

3,4,6-trimethylisoxazolo<3,4-d>pyridazin-7(6H)-one (25505-97-9) → 3-(4-chloro-trans-styryl)-4,6-dimethyl-6H-isoxazolo[3,4-d]pyridazin-7-one (59761-65-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 62 percent / NaOMe / methanol / 0.03 h / Heating

2: 62 percent / sulphuric acid / 1 h / Ambient temperature

With sulfuric acid; sodium methylate; In methanol;

DOI:10.3987/R-1986-12-3467

Reference yield:

4-chlorobenzaldehyde (104-88-1) → 3-(4-chloro-trans-styryl)-4,6-dimethyl-6H-isoxazolo[3,4-d]pyridazin-7-one (59761-65-8)

Guidance literature:

Multi-step reaction with 2 steps

1: 62 percent / NaOMe / methanol / 0.03 h / Heating

2: 62 percent / sulphuric acid / 1 h / Ambient temperature

With sulfuric acid; sodium methylate; In methanol;

DOI:10.3987/R-1986-12-3467

upstream raw materials:

3,4,6-trimethylisoxazolo<3,4-d>pyridazin-7(6H)-one

4-chlorobenzaldehyde

3-[2-(4-Chloro-phenyl)-2-hydroxy-ethyl]-4,6-dimethyl-6H-isoxazolo[3,4-d]pyridazin-7-one

Downstream raw materials:

5-[(E)-2-(4-Chloro-phenyl)-vinyl]-1,3-dimethyl-1H-pyrazole-4-carbonitrile

7-(4-Chloro-phenyl)-1,3-dimethyl-5-oxo-2,5,6,7-tetrahydro-1H-[1,2]diazepine-4-carbonitrile

C₃₀H₂₄Cl₂N₆O₄

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