6-[Benzyl-((E)-but-2-enyl)-amino]-1,3-dicyclohexyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde

Base Information

Chemical Name:6-[Benzyl-((E)-but-2-enyl)-amino]-1,3-dicyclohexyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde
CAS No.:109519-68-8
Molecular Formula:C₂₈H₃₇N₃O₃
Molecular Weight:463.62
Hs Code.:

Synonyms:6-[Benzyl-((E)-but-2-enyl)-amino]-1,3-dicyclohexyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde

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Chemical Property of 6-[Benzyl-((E)-but-2-enyl)-amino]-1,3-dicyclohexyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde

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Technology Process of 6-[Benzyl-((E)-but-2-enyl)-amino]-1,3-dicyclohexyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde

There total 1 articles about 6-[Benzyl-((E)-but-2-enyl)-amino]-1,3-dicyclohexyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 56.0%

: 107733-62-0
benzyl crotyl amine

: 35825-03-7
6-chloro-1,3-dicyclohexyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde

: 109519-68-8
6-[Benzyl-((E)-but-2-enyl)-amino]-1,3-dicyclohexyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde

Guidance literature:: In ethanol; for 12h; Heating;
DOI:10.1248/cpb.34.3994

Reference yield: 60.0%

: 109519-68-8
6-[Benzyl-((E)-but-2-enyl)-amino]-1,3-dicyclohexyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 109519-76-8
C₃₅H₄₅N₅O₄S

Guidance literature:: With hydrogenchloride; In methanol; at 0 ℃;
DOI:10.1248/cpb.34.3994

Reference yield:

: 109519-68-8
6-[Benzyl-((E)-but-2-enyl)-amino]-1,3-dicyclohexyl-2,4-dioxo-1,2,3,4-tetrahydro-pyrimidine-5-carbaldehyde

: 109519-85-9
(3S,3aS)-5-Benzyl-6,8-dicyclohexyl-3-methyl-2-(toluene-4-sulfonyl)-2,3,3a,4,5,6-hexahydro-1,2,5,6,8-pentaaza-cyclopenta[a]naphthalene-7,9-dione

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / conc. hydrochloric acid / methanol / 0 °C

2: 58 percent / lead tetraacetate / acetonitrile / -5 °C

With lead(IV) acetate; hydrogenchloride; In methanol; acetonitrile;
DOI:10.1248/cpb.34.3994