C₁₀H₁₃NO₂

Base Information

• Chemical Name: C₁₀H₁₃NO₂
• CAS No.: 1229446-61-0
• Molecular Formula: C₁₀H₁₃NO₂
• Molecular Weight: 179.219

Synonyms:C₁₀H₁₃NO₂

Chemical Property of C₁₀H₁₃NO₂

Chemical Property:

Purity/Quality:

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Technology Process of C₁₀H₁₃NO₂

There total 2 articles about C₁₀H₁₃NO₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C10H15NO3 → C10H13NO2 (1229446-61-0)

Guidance literature:

With triethylamine; trifluoroacetic anhydride; In dichloromethane; at -40 - 20 ℃; Inert atmosphere;

DOI:10.1002/chem.201300538

Reference yield:

3-cyclohexylprop-2-ynal (4361-25-5) → C10H13NO2 (1229446-61-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

1.2: 14 h / 0 °C / Inert atmosphere

2.1: trifluoroacetic anhydride; triethylamine / dichloromethane / -40 - 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; triethylamine; trifluoroacetic anhydride; In tetrahydrofuran; dichloromethane; 1.1: |Henry Nitro Aldol Condensation / 1.2: |Henry Nitro Aldol Condensation;

DOI:10.1002/chem.201300538

Reference yield: 74.0%

C10H13NO2 (1229446-61-0) + trimethylaluminum (75-24-1) → (3-methyl-4-nitrobut-1-yn-1-yl)cyclohexane

Guidance literature:

trimethylaluminum; With copper(I) thiophene-2-carboxylate; (R)-(-)-1-[(S)-2-(diphenylphosphino)ferrocene]ethyldicyclohexylphosphine; In diethyl ether; at -10 ℃; for 0.1h; Inert atmosphere;

C₁₀H₁₃NO₂; In diethyl ether; at -10 ℃; for 1h; enantioselective reaction; Inert atmosphere;

DOI:10.1002/chem.201300538

upstream raw materials:

3-cyclohexylprop-2-ynal

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