12-amino-1,3,8,10-tetrabenzyl-1,3,8,10-tetraazadispiro-[4.1.4.2]tridec-12-ene-2,4,9,11-tetraone

Base Information

Chemical Name:12-amino-1,3,8,10-tetrabenzyl-1,3,8,10-tetraazadispiro-[4.1.4.2]tridec-12-ene-2,4,9,11-tetraone
CAS No.:1343490-36-7
Molecular Formula:C₃₇H₃₃N₅O₄
Molecular Weight:611.7
Hs Code.:

Synonyms:12-amino-1,3,8,10-tetrabenzyl-1,3,8,10-tetraazadispiro-[4.1.4.2]tridec-12-ene-2,4,9,11-tetraone

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Chemical Property of 12-amino-1,3,8,10-tetrabenzyl-1,3,8,10-tetraazadispiro-[4.1.4.2]tridec-12-ene-2,4,9,11-tetraone

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Technology Process of 12-amino-1,3,8,10-tetrabenzyl-1,3,8,10-tetraazadispiro-[4.1.4.2]tridec-12-ene-2,4,9,11-tetraone

There total 8 articles about 12-amino-1,3,8,10-tetrabenzyl-1,3,8,10-tetraazadispiro-[4.1.4.2]tridec-12-ene-2,4,9,11-tetraone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 773837-37-9
sodium cyanide

: 120803-26-1
1,3-dibenzyl-5-methyleneimidazolidine-2,4-dione

: 1343490-34-5
(1,3-dibenzyl-2,5-dioxoimidazolidin-4-yl)acetonitrile

: 1343490-36-7
12-amino-1,3,8,10-tetrabenzyl-1,3,8,10-tetraazadispiro-[4.1.4.2]tridec-12-ene-2,4,9,11-tetraone

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); In water; acetonitrile; at 40 ℃; for 4h;
DOI:10.1016/j.tet.2011.09.034

Reference yield:

: 773837-37-9
sodium cyanide

: 120803-26-1
1,3-dibenzyl-5-methyleneimidazolidine-2,4-dione

: 1343490-36-7
12-amino-1,3,8,10-tetrabenzyl-1,3,8,10-tetraazadispiro-[4.1.4.2]tridec-12-ene-2,4,9,11-tetraone

Guidance literature:: With copper(II) bis(trifluoromethanesulfonate); In water; acetonitrile; at 40 ℃; for 14h;
DOI:10.1016/j.tet.2011.09.034

Reference yield:

: 16935-43-6
1,3-dibenzylimidazolidine-2,4-dione

: 1343490-36-7
12-amino-1,3,8,10-tetrabenzyl-1,3,8,10-tetraazadispiro-[4.1.4.2]tridec-12-ene-2,4,9,11-tetraone

Guidance literature:: Multi-step reaction with 2 steps

1: ethanolamine / tetrahydrofuran / 24 h / 80 °C

2: copper(II) bis(trifluoromethanesulfonate) / water; acetonitrile / 14 h / 40 °C

With copper(II) bis(trifluoromethanesulfonate); ethanolamine; In tetrahydrofuran; water; acetonitrile;
DOI:10.1016/j.tet.2011.09.034