(3-Benzyloxyl-2,12,13-trimethoxyl)-5,6,7,9-tetrahydro indolo[2,3-e][3]benzazocin-8-one

Base Information

Chemical Name:(3-Benzyloxyl-2,12,13-trimethoxyl)-5,6,7,9-tetrahydro indolo[2,3-e][3]benzazocin-8-one
CAS No.:1415027-00-7
Molecular Formula:C₂₇H₂₆N₂O₅
Molecular Weight:458.514
Hs Code.:

Synonyms:(3-Benzyloxyl-2,12,13-trimethoxyl)-5,6,7,9-tetrahydro indolo[2,3-e][3]benzazocin-8-one

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Chemical Property of (3-Benzyloxyl-2,12,13-trimethoxyl)-5,6,7,9-tetrahydro indolo[2,3-e][3]benzazocin-8-one

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Technology Process of (3-Benzyloxyl-2,12,13-trimethoxyl)-5,6,7,9-tetrahydro indolo[2,3-e][3]benzazocin-8-one

There total 3 articles about (3-Benzyloxyl-2,12,13-trimethoxyl)-5,6,7,9-tetrahydro indolo[2,3-e][3]benzazocin-8-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 54.0%

: 1415026-84-4
5-amido-6-(2',3'-dimethoxylphenyl)-9-benzyloxy-8-methoxy-1,2-dihydrobenzo[d]azocin-4-one

: 1415027-00-7
(3-Benzyloxyl-2,12,13-trimethoxyl)-5,6,7,9-tetrahydro indolo[2,3-e][3]benzazocin-8-one

Guidance literature:: 5-amido-6-(2',3'-dimethoxylphenyl)-9-benzyloxy-8-methoxy-1,2-dihydrobenzo[d]azocin-4-one; With palladium(II) trifluoroacetate; oxygen; copper diacetate; In dimethyl sulfoxide; at 70 - 80 ℃; for 22h;

With sodium hydroxide; In water; at 20 ℃; for 0.0833333h;
DOI:10.1016/j.tet.2012.10.011 DOI:10.1016/j.tet.2012.10.011

Reference yield:

: 36455-21-7
3-benzyloxy-4-methoxyphenylethylamine

: 1415027-00-7
(3-Benzyloxyl-2,12,13-trimethoxyl)-5,6,7,9-tetrahydro indolo[2,3-e][3]benzazocin-8-one

Guidance literature:: Multi-step reaction with 3 steps

2.1: acetonitrile / Reflux

3.1: palladium(II) trifluoroacetate; copper diacetate; oxygen / dimethyl sulfoxide / 22 h / 70 - 80 °C

3.2: 0.08 h / 20 °C

With palladium(II) trifluoroacetate; oxygen; copper diacetate; In dimethyl sulfoxide; acetonitrile; 1.1: |Bischler-Napieralski Reaction;
DOI:10.1016/j.tet.2012.10.011 DOI:10.1016/j.tet.2012.10.011

Reference yield:

: 1521-38-6
2,3-dimethoxybenzoic acid

: 1415027-00-7
(3-Benzyloxyl-2,12,13-trimethoxyl)-5,6,7,9-tetrahydro indolo[2,3-e][3]benzazocin-8-one

Guidance literature:: Multi-step reaction with 3 steps

2.1: acetonitrile / Reflux

3.1: palladium(II) trifluoroacetate; copper diacetate; oxygen / dimethyl sulfoxide / 22 h / 70 - 80 °C

3.2: 0.08 h / 20 °C

With palladium(II) trifluoroacetate; oxygen; copper diacetate; In dimethyl sulfoxide; acetonitrile; 1.1: |Bischler-Napieralski Reaction;
DOI:10.1016/j.tet.2012.10.011 DOI:10.1016/j.tet.2012.10.011