Technology Process of N6-benzoyladenine
There total 13 articles about N6-benzoyladenine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-benzoyladenine;
In
diphenylether;
for 0.0333333h;
Heating;
DOI:10.1021/ol0167210
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: N,O-bis(trimethylsilyl)acetamide / acetonitrile / 0.5 h / 80 °C
1.2: 75 percent / Me3SiOTf / acetonitrile / 1.5 h / 80 °C
2.1: 90 percent / m-CPBA; NaHCO3 / CH2Cl2 / 0.5 h / 0 °C
3.1: 61 percent / N-benzoyladenine / diphenyl ether / 0.03 h / Heating
With
N,O-bis-(trimethylsilyl)-acetamide; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; N-benzoyladenine;
In
diphenylether; dichloromethane; acetonitrile;
DOI:10.1021/ol0167210
- Guidance literature:
-
Multi-step reaction with 7 steps
1.1: LiN(SiMe3)2 / diethyl ether / 0.25 h / -78 °C
1.2: 86 percent / tetrahydrofuran; diethyl ether / -78 - 20 °C
2.1: 33 percent / n-Bu3SnH; AIBN / benzene / 6 h / 80 °C
3.1: 30 percent / AIBN; NaHCO3 / CHCl3 / 36 h / Heating
4.1: H2SO4 / acetic acid; CH2Cl2 / 7 h / 20 °C
5.1: N,O-bis(trimethylsilyl)acetamide / acetonitrile / 0.5 h / 80 °C
5.2: 75 percent / Me3SiOTf / acetonitrile / 1.5 h / 80 °C
6.1: 90 percent / m-CPBA; NaHCO3 / CH2Cl2 / 0.5 h / 0 °C
7.1: 61 percent / N-benzoyladenine / diphenyl ether / 0.03 h / Heating
With
N,O-bis-(trimethylsilyl)-acetamide; 2,2'-azobis(isobutyronitrile); sulfuric acid; tri-n-butyl-tin hydride; sodium hydrogencarbonate; 3-chloro-benzenecarboperoxoic acid; N-benzoyladenine; lithium hexamethyldisilazane;
In
diphenylether; diethyl ether; dichloromethane; chloroform; acetic acid; acetonitrile; benzene;
DOI:10.1021/ol0167210
![(2S,3S,3aR,5R,6R,6aS)-6-Acetoxy-3-benzenesulfinyl-5-(6-benzoylamino-purin-9-yl)-2-ethoxycarbonylmethyl-hexahydro-furo[3,2-b]furan-2-carboxylic acid ethyl ester](/Databaselist/images/loading.webp)
