C₇₈H₁₀₈N₂O₁₁Si₂

Base Information

Chemical Name:C₇₈H₁₀₈N₂O₁₁Si₂
CAS No.:591231-40-2
Molecular Formula:C₇₈H₁₀₈N₂O₁₁Si₂
Molecular Weight:1305.89
Hs Code.:

C<sub>78</sub>H<sub>108</sub>N<sub>2</sub>O<sub>11</sub>Si<sub>2</sub>

Synonyms:C₇₈H₁₀₈N₂O₁₁Si₂

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Chemical Property of C₇₈H₁₀₈N₂O₁₁Si₂

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Technology Process of C₇₈H₁₀₈N₂O₁₁Si₂

There total 12 articles about C₇₈H₁₀₈N₂O₁₁Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 183788-34-3
C₅₁H₇₃O₇Si₂NOCH₃NH₂

: 591231-39-9
C₂₇H₃₇N₃O₅

: 591231-40-2
C₇₈H₁₀₈N₂O₁₁Si₂

Guidance literature:: With polyvinylpyridine; dibutyltin chloride; In benzene; for 4.5h; Heating;
DOI:10.1021/ol034894e

Reference yield:

: 434283-57-5
C₂₉H₄₀O₇

: 591231-40-2
C₇₈H₁₀₈N₂O₁₁Si₂

Guidance literature:: Multi-step reaction with 8 steps

1: 98 percent / Zn; acetic acid / CH₂Cl₂ / 0.5 h / Heating

2: 93 percent / HCl / CH₂Cl₂; diethyl ether / 3.5 h / 0 °C

3: 74 percent / Ag₂O / tetrahydrofuran; H₂O / 2 h / 70 - 75 °C

4: DIBAL-H / CH₂Cl₂; toluene / 3 h / -78 °C

5: 27 mg / 4-methylmorpholine N-oxide; 4 Angstroem molecular sieves; tetrapropylammonium perruthenate / CH₂Cl₂ / 3 h / 20 °C

6: 75 percent / PTAB; HBr / tetrahydrofuran; acetic acid / 0.17 h / 0 °C

7: 81 percent / tetramethylguanidinium azide / nitromethane / 0 - 20 °C

8: 71 percent / dibutyltindichloride; polyvinylpyridine / benzene / 4.5 h / Heating

With hydrogenchloride; polyvinylpyridine; tetrapropylammonium perruthennate; PTAB; 4 A molecular sieve; dibutyltin chloride; hydrogen bromide; diisobutylaluminium hydride; acetic acid; 4-methylmorpholine N-oxide; tetramethylguanidinum azide; silver(l) oxide; zinc; In tetrahydrofuran; diethyl ether; nitromethane; dichloromethane; water; acetic acid; toluene; benzene;
DOI:10.1021/ol034894e

Reference yield:

: 434283-40-6
C₂₉H₄₀O₅

: 591231-40-2
C₇₈H₁₀₈N₂O₁₁Si₂

Guidance literature:: Multi-step reaction with 6 steps

1: 2,2,2,3'-tetrafluoroacetophenone; Oxone; NaHCO₃ / acetonitrile; various solvent(s); H₂O / 1 h / cooling

2: DIBAL-H / CH₂Cl₂; toluene / 3 h / -78 °C

3: 27 mg / 4-methylmorpholine N-oxide; 4 Angstroem molecular sieves; tetrapropylammonium perruthenate / CH₂Cl₂ / 3 h / 20 °C

4: 75 percent / PTAB; HBr / tetrahydrofuran; acetic acid / 0.17 h / 0 °C

5: 81 percent / tetramethylguanidinium azide / nitromethane / 0 - 20 °C

6: 71 percent / dibutyltindichloride; polyvinylpyridine / benzene / 4.5 h / Heating

With Oxone; polyvinylpyridine; tetrapropylammonium perruthennate; 2,2,2,3'-tetrafluoroacetophenone; PTAB; 4 A molecular sieve; dibutyltin chloride; hydrogen bromide; diisobutylaluminium hydride; sodium hydrogencarbonate; 4-methylmorpholine N-oxide; tetramethylguanidinum azide; In tetrahydrofuran; nitromethane; dichloromethane; water; acetic acid; toluene; acetonitrile; benzene;
DOI:10.1021/ol034894e