2-acetamido-4,6-di-O-benzoyl-2-deoxy-3-O-p,p'-dimethoxytrityl-α-D-glucopyranose

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Chemical Name:2-acetamido-4,6-di-O-benzoyl-2-deoxy-3-O-p,p'-dimethoxytrityl-α-D-glucopyranose
CAS No.:141334-46-5
Molecular Formula:C₄₃H₄₁NO₁₀
Molecular Weight:731.799
Hs Code.:

Synonyms:2-acetamido-4,6-di-O-benzoyl-2-deoxy-3-O-p,p'-dimethoxytrityl-α-D-glucopyranose

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Chemical Property of 2-acetamido-4,6-di-O-benzoyl-2-deoxy-3-O-p,p'-dimethoxytrityl-α-D-glucopyranose

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Technology Process of 2-acetamido-4,6-di-O-benzoyl-2-deoxy-3-O-p,p'-dimethoxytrityl-α-D-glucopyranose

There total 5 articles about 2-acetamido-4,6-di-O-benzoyl-2-deoxy-3-O-p,p'-dimethoxytrityl-α-D-glucopyranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.0%

: 141334-44-3
2-acetamido-1,4,6-tri-O-benzoyl-2-deoxy-3-O-p,p'-dimethoxytrityl-α-D-glucopyranose

: 141334-46-5
2-acetamido-4,6-di-O-benzoyl-2-deoxy-3-O-p,p'-dimethoxytrityl-α-D-glucopyranose

Guidance literature:: With dimethyl amine; In acetonitrile; at 20 ℃; for 48h;
DOI:10.1016/0008-6215(93)80024-9

Reference yield:

: 16730-89-5
Benzyl 2-acetamido-3-O-acetyl-2-deoxy-α-D-glucopyranoside

: 141334-46-5
2-acetamido-4,6-di-O-benzoyl-2-deoxy-3-O-p,p'-dimethoxytrityl-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / 10percent Pd-C / methanol / 8 h / 20 °C

2: pyridine / 16 h / 20 °C

3: 60 percent / acetyl chloride, methanol / 1) 1 deg C, 12 h, 2) 20 deg C, 7 h

4: 70 percent / 2,4,6-collidine / CH₂Cl₂ / 72 h / 20 °C

5: 62 percent / Me₂NH / acetonitrile / 48 h / 20 °C

With pyridine; 2,4,6-trimethyl-pyridine; methanol; hydrogen; dimethyl amine; acetyl chloride; palladium on activated charcoal; In methanol; dichloromethane; acetonitrile;
DOI:10.1016/0008-6215(93)80024-9

Reference yield:

: 51449-95-7
(+)-2-acetamido-3-O-acetyl-2-deoxy-β-D-glucopyranoside

: 141334-46-5
2-acetamido-4,6-di-O-benzoyl-2-deoxy-3-O-p,p'-dimethoxytrityl-α-D-glucopyranose

Guidance literature:: Multi-step reaction with 4 steps

1: pyridine / 16 h / 20 °C

2: 60 percent / acetyl chloride, methanol / 1) 1 deg C, 12 h, 2) 20 deg C, 7 h

3: 70 percent / 2,4,6-collidine / CH₂Cl₂ / 72 h / 20 °C

4: 62 percent / Me₂NH / acetonitrile / 48 h / 20 °C

With pyridine; 2,4,6-trimethyl-pyridine; methanol; dimethyl amine; acetyl chloride; In dichloromethane; acetonitrile;
DOI:10.1016/0008-6215(93)80024-9