N⁷-(4-chlorophenoxyethyl)-3'-O-methylguanosine 5'-monophosphate triethylammonium salt

Base Information

• Chemical Name: N⁷-(4-chlorophenoxyethyl)-3'-O-methylguanosine 5'-monophosphate triethylammonium salt
• CAS No.: 1447816-96-7
• Molecular Formula: C₆H₁₅N*C₁₉H₂₃ClN₅O₉P
• Molecular Weight: 633.038

Synonyms:N⁷-(4-chlorophenoxyethyl)-3'-O-methylguanosine 5'-monophosphate triethylammonium salt

Chemical Property of N⁷-(4-chlorophenoxyethyl)-3'-O-methylguanosine 5'-monophosphate triethylammonium salt

Chemical Property:

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Technology Process of N⁷-(4-chlorophenoxyethyl)-3'-O-methylguanosine 5'-monophosphate triethylammonium salt

There total 1 articles about N⁷-(4-chlorophenoxyethyl)-3'-O-methylguanosine 5'-monophosphate triethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

1-(2-bromoethoxy)-4-chlorobenzene (2033-76-3) + 3'-O-methylguanosine 5'-monophosphate triethylammonium salt (860605-85-2) → N7-(4-chlorophenoxyethyl)-3'-O-methylguanosine 5'-monophosphate triethylammonium salt (1447816-96-7)

Guidance literature:

In dimethyl sulfoxide; at 55 ℃; for 48h;

DOI:10.1016/j.bmc.2013.05.041

Reference yield:

N7-(4-chlorophenoxyethyl)-3'-O-methylguanosine 5'-monophosphate triethylammonium salt (1447816-96-7) + C10H12N5O5(PO3PO2)(NCHNCHCH)(2-) → N7-(4-chlorophenoxyethyl)-m3'-OG(5')ppp(5')G triethylammonium salt

Guidance literature:

N⁷-(4-chlorophenoxyethyl)-3'-O-methylguanosine 5'-monophosphate triethylammonium salt; C₁₀H₁₂N₅O₅(PO₃PO₂)(NCHNCHCH)^(2-); With zinc(II) chloride; In N,N-dimethyl-formamide; at 4 ℃; for 72h; Inert atmosphere;

With ethylenediaminetetraacetic acid; In water; N,N-dimethyl-formamide;

DOI:10.1016/j.bmc.2013.05.041

upstream raw materials:

1-(2-bromoethoxy)-4-chlorobenzene

3'-O-methylguanosine 5'-monophosphate triethylammonium salt

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