C₂₅H₄₄N₄

Base Information

Chemical Name:C₂₅H₄₄N₄
CAS No.:1260113-65-2
Molecular Formula:C₂₅H₄₄N₄
Molecular Weight:400.651
Hs Code.:

C<sub>25</sub>H<sub>44</sub>N<sub>4</sub>

Synonyms:C₂₅H₄₄N₄

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Chemical Property of C₂₅H₄₄N₄

Chemical Property:

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Technology Process of C₂₅H₄₄N₄

There total 10 articles about C₂₅H₄₄N₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 1260113-66-3
C₂₅H₄₀N₄O₂

: 1260113-65-2
C₂₅H₄₄N₄

Guidance literature:: With dimethyl sulfide borane; In tetrahydrofuran; at 0 ℃; Reflux;
DOI:10.1002/ejoc.201000569

Reference yield:

: 1260113-89-0
1,3-bis(bromomethyl)-5-methyl-2,4,6-triethylbenzene

: 1260113-65-2
C₂₅H₄₄N₄

Guidance literature:: Multi-step reaction with 5 steps

1: sodium azide / N,N-dimethyl-formamide / 24 h / 20 °C

2: sodium azide / N,N-dimethyl-formamide / 24 h / 20 °C

3: tetrahydrofuran / 51 h / 0 °C / Inert atmosphere; Reflux

4: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

5: dimethyl sulfide borane / tetrahydrofuran / 0 °C / Reflux

With sodium azide; dimethyl sulfide borane; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201000569

Reference yield:

: 1260113-91-4
1,3-bis(azidomethyl)-5-methyl-2,4,6-triethylbenzene

: 1260113-65-2
C₂₅H₄₄N₄

Guidance literature:: Multi-step reaction with 4 steps

1: sodium azide / N,N-dimethyl-formamide / 24 h / 20 °C

2: tetrahydrofuran / 51 h / 0 °C / Inert atmosphere; Reflux

3: trifluoroacetic acid / dichloromethane / 2 h / 0 - 20 °C

4: dimethyl sulfide borane / tetrahydrofuran / 0 °C / Reflux

With sodium azide; dimethyl sulfide borane; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1002/ejoc.201000569