(1S,2S)-3-[(4S)-4-tert-butyl-2-oxazolin-2-yl]-1-methoxy-2-methyl-1-phenylpropane

Base Information

Chemical Name:(1S,2S)-3-[(4S)-4-tert-butyl-2-oxazolin-2-yl]-1-methoxy-2-methyl-1-phenylpropane
CAS No.:379690-47-8
Molecular Formula:C₁₈H₂₇NO₂
Molecular Weight:289.418
Hs Code.:

Synonyms:(1S,2S)-3-[(4S)-4-tert-butyl-2-oxazolin-2-yl]-1-methoxy-2-methyl-1-phenylpropane

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Chemical Property of (1S,2S)-3-[(4S)-4-tert-butyl-2-oxazolin-2-yl]-1-methoxy-2-methyl-1-phenylpropane

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Technology Process of (1S,2S)-3-[(4S)-4-tert-butyl-2-oxazolin-2-yl]-1-methoxy-2-methyl-1-phenylpropane

There total 2 articles about (1S,2S)-3-[(4S)-4-tert-butyl-2-oxazolin-2-yl]-1-methoxy-2-methyl-1-phenylpropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: (1SR,2S,3S)-2-[(4S)-4-tert-butyl-2-oxazolin-2-yl]-1-methoxy-3-methyl-1-phenylcyclopropane

: 379690-47-8
(1S,2S)-3-[(4S)-4-tert-butyl-2-oxazolin-2-yl]-1-methoxy-2-methyl-1-phenylpropane

: (1R,2S)-3-[(4S)-4-tert-butyl-2-oxazolin-2-yl]-1-methoxy-2-methyl-1-phenylpropane

Guidance literature:: With hydrogen; triethylamine; 10percent Pd/C; In tetrahydrofuran; at 25 ℃; for 12h; under 760.051 Torr;
DOI:10.1021/ja010719m

Reference yield:

: 191603-51-7
(S)-4-tert-Butyl-2-((E)-propenyl)-4,5-dihydro-oxazole

: 379690-47-8
(1S,2S)-3-[(4S)-4-tert-butyl-2-oxazolin-2-yl]-1-methoxy-2-methyl-1-phenylpropane

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran / 14 h / 60 °C

2: H₂; Et₃N / 10percent Pd/C / tetrahydrofuran / 12 h / 25 °C / 760.05 Torr

With hydrogen; triethylamine; 10percent Pd/C; In tetrahydrofuran;
DOI:10.1021/ja010719m

Reference yield: 71.0%

: 379690-47-8
(1S,2S)-3-[(4S)-4-tert-butyl-2-oxazolin-2-yl]-1-methoxy-2-methyl-1-phenylpropane

: (3S,4S)-4-methoxy-3-methyl-4-phenylbutan-1-ol

Guidance literature:: (1S,2S)-3-[(4S)-4-tert-butyl-2-oxazolin-2-yl]-1-methoxy-2-methyl-1-phenylpropane; With benzyl chloroformate; In dichloromethane;

With diisobutylaluminium hydride; In toluene; at 25 ℃; for 2h; Further stages.;
DOI:10.1021/ja010719m