3-(2,2-Diethoxyethoxy)-4-methylphthaloylimidobenzene

Base Information

Chemical Name:3-(2,2-Diethoxyethoxy)-4-methylphthaloylimidobenzene
CAS No.:185684-96-2
Molecular Formula:C₂₁H₂₃NO₅
Molecular Weight:369.417
Hs Code.:

Synonyms:3-(2,2-Diethoxyethoxy)-4-methylphthaloylimidobenzene

Suppliers and Price of 3-(2,2-Diethoxyethoxy)-4-methylphthaloylimidobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 3-(2,2-Diethoxyethoxy)-4-methylphthaloylimidobenzene

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 3-(2,2-Diethoxyethoxy)-4-methylphthaloylimidobenzene

There total 5 articles about 3-(2,2-Diethoxyethoxy)-4-methylphthaloylimidobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 85-44-9
phthalic anhydride

: 185684-95-1
3-(2,2-Diethoxyethoxy)-4-methylaniline

: 185684-96-2
3-(2,2-Diethoxyethoxy)-4-methylphthaloylimidobenzene

Guidance literature:: In chloroform; at 61 ℃; for 46h;
DOI:10.1016/S0040-4039(96)02181-8 DOI:10.1055/s-2000-8714

Reference yield:

: 185684-93-9
3-(2,2-Diethoxyethoxy)-4-methylnitrobenzene

: 185684-96-2
3-(2,2-Diethoxyethoxy)-4-methylphthaloylimidobenzene

Guidance literature:: Multi-step reaction with 2 steps

1: 99 percent / H₂ / 10 percent Pd/C / methanol / 25 °C

2: 88 percent / CHCl₃ / 46 h / 61 °C

With hydrogen; palladium on activated charcoal; In methanol; chloroform;
DOI:10.1055/s-2000-8714

Reference yield:

: 5428-54-6
2-methyl-5-nitrophenol

: 185684-96-2
3-(2,2-Diethoxyethoxy)-4-methylphthaloylimidobenzene

Guidance literature:: Multi-step reaction with 3 steps

1: 81 percent / K₂CO₃ / dimethylformamide / 3.5 h / 153 °C

2: 99 percent / H₂ / 10 percent Pd/C / methanol / 25 °C

3: 88 percent / CHCl₃ / 46 h / 61 °C

With hydrogen; potassium carbonate; palladium on activated charcoal; In methanol; chloroform; N,N-dimethyl-formamide;
DOI:10.1055/s-2000-8714