Technology Process of C45H47N5O5
There total 12 articles about C45H47N5O5 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
N-ethyl-N,N-diisopropylamine; HATU;
In
N,N-dimethyl-formamide;
at 20 ℃;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: potassium carbonate / tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2 / ethanol; water; dimethyl sulfoxide; toluene / 2 h / 20 - 100 °C / Inert atmosphere
2: hydrogen / palladium on activated charcoal / isopropyl alcohol; toluene / 24 h / 20 °C
3: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 20 °C
With
hydrogen; potassium carbonate; N-ethyl-N,N-diisopropylamine; HATU;
tetrakis(triphenylphosphine) palladium(0); dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH2Cl2; palladium on activated charcoal;
In
ethanol; water; dimethyl sulfoxide; N,N-dimethyl-formamide; isopropyl alcohol; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogen / palladium on activated charcoal / ethanol / 24 h / 2844.39 Torr
2: methanol / 24 h
3: triethylamine / dichloromethane / 0 - 20 °C
4: methanol; water; lithium hydroxide / tetrahydrofuran / 20 °C
5: N-ethyl-N,N-diisopropylamine; HATU / N,N-dimethyl-formamide / 20 °C
With
methanol; water; hydrogen; triethylamine; N-ethyl-N,N-diisopropylamine; HATU; lithium hydroxide;
palladium on activated charcoal;
In
tetrahydrofuran; methanol; ethanol; dichloromethane; N,N-dimethyl-formamide;