ethyl<3-(2,3-dihydro-1,4-dioxin-5-yl)-2,4,4-trimethyl>cyclohex-2-enylbut-2-enedioate

Base Information

Chemical Name:ethyl<3-(2,3-dihydro-1,4-dioxin-5-yl)-2,4,4-trimethyl>cyclohex-2-enylbut-2-enedioate
CAS No.:161084-33-9
Molecular Formula:C₁₉H₂₆O₆
Molecular Weight:350.412
Hs Code.:

Synonyms:ethyl<3-(2,3-dihydro-1,4-dioxin-5-yl)-2,4,4-trimethyl>cyclohex-2-enylbut-2-enedioate

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Chemical Property of ethyl<3-(2,3-dihydro-1,4-dioxin-5-yl)-2,4,4-trimethyl>cyclohex-2-enylbut-2-enedioate

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Technology Process of ethyl<3-(2,3-dihydro-1,4-dioxin-5-yl)-2,4,4-trimethyl>cyclohex-2-enylbut-2-enedioate

There total 2 articles about ethyl<3-(2,3-dihydro-1,4-dioxin-5-yl)-2,4,4-trimethyl>cyclohex-2-enylbut-2-enedioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2459-05-4
(E)-4-ethoxy-4-oxobut-2-enoic acid

: 144646-66-2
2,4,4-trimethyl-3-<(1,4-dioxen-2-yl)>cyclohex-2-en-1-ol

: 161084-33-9
ethyl<3-(2,3-dihydro-1,4-dioxin-5-yl)-2,4,4-trimethyl>cyclohex-2-enylbut-2-enedioate

Guidance literature:: With dmap; dicyclohexyl-carbodiimide; In dichloromethane; at 0 ℃; for 0.5h;

Reference yield:

: 116809-86-0
2,6,6-trimethyl-1-<2-(1,4-dioxenyl)>-1-cyclohexene

: 161084-33-9
ethyl<3-(2,3-dihydro-1,4-dioxin-5-yl)-2,4,4-trimethyl>cyclohex-2-enylbut-2-enedioate

Guidance literature:: Multi-step reaction with 2 steps

1: 60 percent / sodium carbonate, bromine / CH₂Cl₂ / 0.5 h / -70 °C

2: 85 percent / 4-dimethylaminopyridine, dicyclohexylcarbodiimide / CH₂Cl₂ / 0.5 h / 0 °C

With dmap; bromine; sodium carbonate; dicyclohexyl-carbodiimide; In dichloromethane;