methyl 3-[3-[5-[4-(2-methoxyphenyl)piperazin-1-yl]pentyl]-2,4-dioxothieno[3,4-d]pyrimidin-1-yl]propanoate

Base Information

Chemical Name:methyl 3-[3-[5-[4-(2-methoxyphenyl)piperazin-1-yl]pentyl]-2,4-dioxothieno[3,4-d]pyrimidin-1-yl]propanoate
CAS No.:130475-78-4
Molecular Formula:C₂₆H₃₄N₄O₅S
Molecular Weight:514.646
Hs Code.:

Synonyms:methyl 3-[3-[5-[4-(2-methoxyphenyl)piperazin-1-yl]pentyl]-2,4-dioxothieno[3,4-d]pyrimidin-1-yl]propanoate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl 3-[3-[5-[4-(2-methoxyphenyl)piperazin-1-yl]pentyl]-2,4-dioxothieno[3,4-d]pyrimidin-1-yl]propanoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of methyl 3-[3-[5-[4-(2-methoxyphenyl)piperazin-1-yl]pentyl]-2,4-dioxothieno[3,4-d]pyrimidin-1-yl]propanoate

There total 6 articles about methyl 3-[3-[5-[4-(2-methoxyphenyl)piperazin-1-yl]pentyl]-2,4-dioxothieno[3,4-d]pyrimidin-1-yl]propanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: 130475-77-3
3-<4<5(2-methoxyphenyl)piperazin-1-yl>pentyl>thieno<3,4-d>pyrimidine-2-,4-dione

: 292638-85-8,9003-21-8,96-33-3
acrylic acid methyl ester

: 130475-78-4
methyl 3-[3-[5-[4-(2-methoxyphenyl)piperazin-1-yl]pentyl]-2,4-dioxothieno[3,4-d]pyrimidin-1-yl]propanoate

Guidance literature:: With N-benzyl-trimethylammonium hydroxide; In methanol; chloroform; Heating;

Reference yield: 23.0%

: 130475-77-3
3-<4<5(2-methoxyphenyl)piperazin-1-yl>pentyl>thieno<3,4-d>pyrimidine-2-,4-dione

: 130475-78-4
methyl 3-[3-[5-[4-(2-methoxyphenyl)piperazin-1-yl]pentyl]-2,4-dioxothieno[3,4-d]pyrimidin-1-yl]propanoate

Guidance literature:: In N,N-dimethyl-formamide;

Reference yield:

: 69363-85-5
methyl 4-aminothiophene-3-carboxylate

: 130475-78-4
methyl 3-[3-[5-[4-(2-methoxyphenyl)piperazin-1-yl]pentyl]-2,4-dioxothieno[3,4-d]pyrimidin-1-yl]propanoate

Guidance literature:: Multi-step reaction with 4 steps

1: 98 percent / toluene / Ambient temperature

2: Na₂CO₃, NaI / propan-2-ol / Heating

3: aq. 50percent NaOH / methanol / Heating

4: 24 percent / aq. C₆H₅CH₂N(CH₃)3OH / CHCl₃; methanol / Heating

With sodium hydroxide; N-benzyl-trimethylammonium hydroxide; sodium carbonate; sodium iodide; In methanol; chloroform; isopropyl alcohol; toluene;