C₄₈H₃₀N₆O₆

Base Information

• Chemical Name: C₄₈H₃₀N₆O₆
• CAS No.: 1450813-00-9
• Molecular Formula: C₄₈H₃₀N₆O₆
• Molecular Weight: 786.803
• Mol file: 1450813-00-9.mol

Synonyms:C₄₈H₃₀N₆O₆

Chemical Property of C₄₈H₃₀N₆O₆

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
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MSDS Files:

Useful:

Technology Process of C₄₈H₃₀N₆O₆

There total 2 articles about C₄₈H₃₀N₆O₆ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 25.8%

2,2'-dihydroxybenzil (85-26-7) + benzenehexamine (4444-26-2) → C48H30N6O6 (1450813-00-9)

Guidance literature:

With acetic acid; for 24h; Reflux; Inert atmosphere;

DOI:10.1016/j.tetlet.2013.07.021

Reference yield:

salicylaldehyde (90-02-8) → C48H30N6O6 (1450813-00-9)

Guidance literature:

Multi-step reaction with 3 steps

1: 1,8-diazabicyclo[5.4.0]undec-7-ene; vitamin B₁ / dimethyl sulfoxide / 5 h / 60 °C / Inert atmosphere

2: triethylamine; copper(ll) sulfate pentahydrate / acetonitrile; water / 0.17 h / 85 °C

3: acetic acid / 24 h / Reflux; Inert atmosphere

With copper(ll) sulfate pentahydrate; vitamin B₁; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; triethylamine; In water; dimethyl sulfoxide; acetonitrile; 1: |Benzoin Condensation;

DOI:10.1016/j.tetlet.2013.07.021

upstream raw materials:

salicylaldehyde

2,2'-dihydroxybenzil

benzenehexamine