5-[[(2-methoxypyridin-4-yl)amino]methylidene]-2,2-dimethyl-1,3-dioxane-4,6-dione

Base Information

Chemical Name:5-[[(2-methoxypyridin-4-yl)amino]methylidene]-2,2-dimethyl-1,3-dioxane-4,6-dione
CAS No.:1018812-92-4
Molecular Formula:C₁₃H₁₄N₂O₅
Molecular Weight:278.265
Hs Code.:

Synonyms:5-[[(2-methoxypyridin-4-yl)amino]methylidene]-2,2-dimethyl-1,3-dioxane-4,6-dione

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Chemical Property of 5-[[(2-methoxypyridin-4-yl)amino]methylidene]-2,2-dimethyl-1,3-dioxane-4,6-dione

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Technology Process of 5-[[(2-methoxypyridin-4-yl)amino]methylidene]-2,2-dimethyl-1,3-dioxane-4,6-dione

There total 1 articles about 5-[[(2-methoxypyridin-4-yl)amino]methylidene]-2,2-dimethyl-1,3-dioxane-4,6-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 20265-39-8
4-amino-2-methoxypyridine

: 15568-85-1
5-methoxymethylene-2,2-dimethyl-1,3-dioxane-4,6-dione

: 1018812-92-4
5-[[(2-methoxypyridin-4-yl)amino]methylidene]-2,2-dimethyl-1,3-dioxane-4,6-dione

Guidance literature:: In isopropyl alcohol; Heating;
DOI:10.1016/j.tet.2008.01.055

Reference yield:

: 1018812-92-4
5-[[(2-methoxypyridin-4-yl)amino]methylidene]-2,2-dimethyl-1,3-dioxane-4,6-dione

: C₂₂H₁₂F₅N₃O₃

Guidance literature:: Multi-step reaction with 3 steps

1: 0.5 h / 220 °C

2: sodium hydride / 4 h / 150 °C / Microwave irradiation

3: hydrogenchloride / water / 1 h / 90 °C

With hydrogenchloride; sodium hydride; In water;
DOI:10.1016/j.bmcl.2016.04.042

Reference yield:

: 1018812-92-4
5-[[(2-methoxypyridin-4-yl)amino]methylidene]-2,2-dimethyl-1,3-dioxane-4,6-dione

: C₁₅H₈F₃N₃O₄

Guidance literature:: Multi-step reaction with 3 steps

1: 0.5 h / 220 °C

2: sodium hydride / 4 h / 150 °C / Microwave irradiation

3: hydrogenchloride / water / 1 h / 90 °C

With hydrogenchloride; sodium hydride; In water;
DOI:10.1016/j.bmcl.2016.04.042