3,8-Dibenzyl-2,2,7,7-tetraphenoxy-1,3,6,8-tetraaza-2λ⁵,7λ⁵-diphospha-tricyclo[5.3.0.0^2,6]decane-4,9-dione

Base Information

• Chemical Name: 3,8-Dibenzyl-2,2,7,7-tetraphenoxy-1,3,6,8-tetraaza-2λ⁵,7λ⁵-diphospha-tricyclo[5.3.0.0^2,6]decane-4,9-dione
• CAS No.: 106585-47-1
• Molecular Formula: C₄₂H₃₈N₄O₆P₂
• Molecular Weight: 756.734

Synonyms:3,8-Dibenzyl-2,2,7,7-tetraphenoxy-1,3,6,8-tetraaza-2λ⁵,7λ⁵-diphospha-tricyclo[5.3.0.0^2,6]decane-4,9-dione

Chemical Property of 3,8-Dibenzyl-2,2,7,7-tetraphenoxy-1,3,6,8-tetraaza-2λ⁵,7λ⁵-diphospha-tricyclo[5.3.0.0^2,6]decane-4,9-dione

Chemical Property:

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Technology Process of 3,8-Dibenzyl-2,2,7,7-tetraphenoxy-1,3,6,8-tetraaza-2λ⁵,7λ⁵-diphospha-tricyclo[5.3.0.0^2,6]decane-4,9-dione

There total 1 articles about 3,8-Dibenzyl-2,2,7,7-tetraphenoxy-1,3,6,8-tetraaza-2λ⁵,7λ⁵-diphospha-tricyclo[5.3.0.0^2,6]decane-4,9-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

(2-Azido-acetyl)-benzyl-phosphoramidic acid diphenyl ester (106585-38-0) → 3,8-Dibenzyl-2,2,7,7-tetraphenoxy-1,3,6,8-tetraaza-2λ5,7λ5-diphospha-tricyclo[5.3.0.02,6]decane-4,9-dione (106585-47-1) + Triphenylphosphine oxide (791-28-6)

Guidance literature:

With triphenylphosphine; In dichloromethane; Yield given;

Reference yield: 50.0%

3,8-Dibenzyl-2,2,7,7-tetraphenoxy-1,3,6,8-tetraaza-2λ5,7λ5-diphospha-tricyclo[5.3.0.02,6]decane-4,9-dione (106585-47-1) → Gly-NHBzl*HBr

Guidance literature:

With hydrogen bromide; In acetic acid;

upstream raw materials:

(2-Azido-acetyl)-benzyl-phosphoramidic acid diphenyl ester

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