N₄,2',3'-O,O-tribenzoylcytidin-5'-yl hydrogenophosphonate, triethylammonium salt

Base Information

• Chemical Name: N₄,2',3'-O,O-tribenzoylcytidin-5'-yl hydrogenophosphonate, triethylammonium salt
• CAS No.: 1058150-71-2
• Molecular Formula: C₆H₁₅N*C₃₀H₂₆N₃O₁₀P
• Molecular Weight: 720.716

Synonyms:N₄,2',3'-O,O-tribenzoylcytidin-5'-yl hydrogenophosphonate, triethylammonium salt

Chemical Property of N₄,2',3'-O,O-tribenzoylcytidin-5'-yl hydrogenophosphonate, triethylammonium salt

Chemical Property:

Purity/Quality:

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Technology Process of N₄,2',3'-O,O-tribenzoylcytidin-5'-yl hydrogenophosphonate, triethylammonium salt

There total 1 articles about N₄,2',3'-O,O-tribenzoylcytidin-5'-yl hydrogenophosphonate, triethylammonium salt which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C36H30N3O10P + triethylamine (121-44-8) → N4,2',3'-O,O-tribenzoylcytidin-5'-yl hydrogenophosphonate, triethylammonium salt (1058150-71-2)

Guidance literature:

With pyridine; water; for 0.166667h; Inert atmosphere;

DOI:10.1021/jm800617c

Reference yield:

thiophosphoric acid O,O'-bis-(2-cyano-1,1-dimethyl-ethyl) ester O''-[3-hydroxy-5-(2-isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-4-methoxy-tetrahydro-furan-2-ylmethyl] ester + N4,2',3'-O,O-tribenzoylcytidin-5'-yl hydrogenophosphonate, triethylammonium salt (1058150-71-2) → O-(N4,2',3'-O,O-tribenzoylcytidin-5'-yl)-O-{N2-isobutyryl-2'-O-methyl-5'-O-[bis-(2-cyano-1,1-dimethylethyl)thionophosphoryl]guanosin-3'-yl} hydrogenophosphonate diester (1058150-83-6)

Guidance literature:

With pyridine; PS acyl chloride resin; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/jm800617c

Reference yield:

phosphoric acid bis-(2-cyano-ethyl) ester 3-hydroxy-5-(2-isobutyrylamino-6-oxo-1,6-dihydro-purin-9-yl)-4-methoxy-tetrahydro-furan-2-ylmethyl ester + N4,2',3'-O,O-tribenzoylcytidin-5'-yl hydrogenophosphonate, triethylammonium salt (1058150-71-2) → O-(N4,2',3'-O,O-tribenzoylcytidin-5'-yl)-O-{N2-isobutyryl-2'-O-methyl-5'-O-[bis-(2-cyanoethyl)phosphoryl]guanosin-3'-yl} hydrogenphosphonate diester (1058150-76-7)

Guidance literature:

With pyridine; PS acyl chloride resin; In dichloromethane; at 20 ℃; for 2h;

DOI:10.1021/jm800617c

upstream raw materials:

triethylamine

Downstream raw materials:

O-(N₄,2',3'-O,O-tribenzoylcytidin-5'-yl)-O-{N₂-isobutyryl-2'-O-methyl-5'-O-[bis-(2-cyanoethyl)phosphoryl]guanosin-3'-yl} hydrogenphosphonate diester

O-(N₄,2',3'-O,O-tribenzoylcytidin-5'-yl)-O-{N₂-isobutyryl-2'-O-methyl-5'-O-[bis-(2-cyano-1,1-dimethylethyl)thionophosphoryl]guanosin-3'-yl} hydrogenophosphonate diester

O-(N₄,2',3'-O,O-tribenzoylcytidin-5'-yl)-O-[N₂-isobutyryl-2'-O-methyl-5'-O-(4,4'-dimethoxytrityl)guanosin-3'-yl] hydrogenophosphonate diester

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