Dimethyl (4-chloro-2-phenylpyrrolo-<3,2-d>-pyrimidine-7-yl)methyleneammonium chloride

Base Information

Chemical Name:Dimethyl (4-chloro-2-phenylpyrrolo-<3,2-d>-pyrimidine-7-yl)methyleneammonium chloride
CAS No.:75682-08-5
Molecular Formula:C₁₅H₁₄ClN₄*Cl
Molecular Weight:321.209
Hs Code.:

Synonyms:Dimethyl (4-chloro-2-phenylpyrrolo-<3,2-d>-pyrimidine-7-yl)methyleneammonium chloride

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Chemical Property of Dimethyl (4-chloro-2-phenylpyrrolo-<3,2-d>-pyrimidine-7-yl)methyleneammonium chloride

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Technology Process of Dimethyl (4-chloro-2-phenylpyrrolo-<3,2-d>-pyrimidine-7-yl)methyleneammonium chloride

There total 1 articles about Dimethyl (4-chloro-2-phenylpyrrolo-<3,2-d>-pyrimidine-7-yl)methyleneammonium chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 72168-62-8
5-Amino-6-methyl-4-oxo-2-phenyl-3,4-dihydropyrimidine

: 75682-08-5
Dimethyl (4-chloro-2-phenylpyrrolo-<3,2-d>-pyrimidine-7-yl)methyleneammonium chloride

Guidance literature:: With trichlorophosphate; In N,N-dimethyl-formamide; at 80 ℃; for 1h;
DOI:10.1007/BF00773110

Reference yield: 63.0%

: 75682-08-5
Dimethyl (4-chloro-2-phenylpyrrolo-<3,2-d>-pyrimidine-7-yl)methyleneammonium chloride

: 75682-07-4
4-Chloro-2-phenylpyrrolo<3,2-d>-pyrimidine-7-carboxaldehyde

Guidance literature:: With sodium hydrogencarbonate; In water;
DOI:10.1007/BF00773110

Reference yield:

: 75682-08-5
Dimethyl (4-chloro-2-phenylpyrrolo-<3,2-d>-pyrimidine-7-yl)methyleneammonium chloride

: 75682-11-0
4-Chloro-2-phenylpyrrolo<3,2-d>pyrimidine-7-carboxaldehyde phenylhydrazone

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / NaHCO₃ / H₂O

2: 61.6 percent / conc. aq. HCl / aq. ethanol / 1 h / Heating

With hydrogenchloride; sodium hydrogencarbonate; In ethanol; water;
DOI:10.1007/BF00773110