N-[3-(tert-butyl(dimethyl)silyloxy)-1-propynyl]-N-phenylcarbamic acid methyl ester

Base Information

Chemical Name:N-[3-(tert-butyl(dimethyl)silyloxy)-1-propynyl]-N-phenylcarbamic acid methyl ester
CAS No.:865081-72-7
Molecular Formula:C₁₇H₂₅NO₃Si
Molecular Weight:319.476
Hs Code.:

Synonyms:N-[3-(tert-butyl(dimethyl)silyloxy)-1-propynyl]-N-phenylcarbamic acid methyl ester

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Chemical Property of N-[3-(tert-butyl(dimethyl)silyloxy)-1-propynyl]-N-phenylcarbamic acid methyl ester

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Technology Process of N-[3-(tert-butyl(dimethyl)silyloxy)-1-propynyl]-N-phenylcarbamic acid methyl ester

There total 1 articles about N-[3-(tert-butyl(dimethyl)silyloxy)-1-propynyl]-N-phenylcarbamic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 35.0%

: 2603-10-3
N-phenyl methyl carbamate

: 138376-12-2
((3-bromoprop-2-yn-1-yl)oxy)(tert-butyl)dimethylsilane

: 865081-72-7
N-[3-(tert-butyl(dimethyl)silyloxy)-1-propynyl]-N-phenylcarbamic acid methyl ester

Guidance literature:: With potassium hexamethylsilazane; copper(l) iodide; 1,10-Phenanthroline; In toluene; at 90 ℃; for 12h;
DOI:10.1021/ol0512841

Reference yield: 65.0%

: 865081-72-7
N-[3-(tert-butyl(dimethyl)silyloxy)-1-propynyl]-N-phenylcarbamic acid methyl ester

: 865081-75-0
N-(3-hydroxy-1-propynyl)-N-phenylcarbamic acid methyl ester

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at -78 - -20 ℃;
DOI:10.1021/ol0512841 DOI:10.1016/j.tet.2005.11.081

Reference yield: 32.0%

: 865081-72-7
N-[3-(tert-butyl(dimethyl)silyloxy)-1-propynyl]-N-phenylcarbamic acid methyl ester

: 498-66-8
norborn-2-ene

: ((1S,2R,5S,6R)-4-Hydroxymethyl-tricyclo[4.2.1.0^2,5]non-3-en-3-yl)-phenyl-carbamic acid methyl ester

Guidance literature:: With chloro(1,5-cyclooctadiene)(pentamethylcyclopentadiene)ruthenium(II); In tetrahydrofuran; at 60 ℃; for 72h;
DOI:10.1016/j.tet.2005.11.081