C₁₈H₂₄O₄

Base Information

Chemical Name:C₁₈H₂₄O₄
CAS No.:1373516-88-1
Molecular Formula:C₁₈H₂₄O₄
Molecular Weight:304.386
Hs Code.:

C<sub>18</sub>H<sub>24</sub>O<sub>4</sub>

Synonyms:C₁₈H₂₄O₄

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Chemical Property of C₁₈H₂₄O₄

Chemical Property:

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Technology Process of C₁₈H₂₄O₄

There total 9 articles about C₁₈H₂₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1373516-87-0
C₁₈H₂₅IO₄

: 1373516-88-1
C₁₈H₂₄O₄

Guidance literature:: With potassium tert-butylate; In tetrahydrofuran; at 0 ℃; for 0.666667h;
DOI:10.1021/ja300565t

Reference yield:

: 1021700-94-6
C₁₉H₂₈O₅Si

: 1373516-88-1
C₁₈H₂₄O₄

Guidance literature:: Multi-step reaction with 9 steps

1.1: sodium hexamethyldisilazane / tetrahydrofuran / 1 h / 0 °C

1.2: 2 h / 0 °C

2.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C

3.1: bis(1,5-cyclooctadiene)diiridium(I) dichloride; sodium carbonate / toluene / 10 h / 100 °C

4.1: tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride / benzene / 16 h / 60 °C / Inert atmosphere

5.1: palladium on activated charcoal; hydrogen / tetrahydrofuran; ethanol / 72 h / 20 °C

6.1: pyridinium p-toluenesulfonate / dichloromethane / 3.5 h / 20 °C

7.1: diisobutylaluminium hydride / hexane; dichloromethane / 3.17 h / -40 - 0 °C

8.1: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 1 h / 20 °C

9.1: potassium tert-butylate / tetrahydrofuran / 0.67 h / 0 °C

With 1H-imidazole; tricyclohexylphosphine[1,3-bis(2,4,6-trimethylphenyl)-4,5-dihydroimidazol-2-ylidine][benzylidene]ruthenium(II) dichloride; bis(1,5-cyclooctadiene)diiridium(I) dichloride; palladium on activated charcoal; potassium tert-butylate; tetrabutyl ammonium fluoride; hydrogen; iodine; sodium hexamethyldisilazane; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; sodium carbonate; triphenylphosphine; In tetrahydrofuran; ethanol; hexane; dichloromethane; toluene; benzene; 1.1: Wittig reaction / 1.2: Wittig reaction;
DOI:10.1021/ja300565t

Reference yield:

: C₁₀H₁₈O₄

: 1373516-88-1
C₁₈H₂₄O₄

Guidance literature:: Multi-step reaction with 4 steps

1: pyridinium p-toluenesulfonate / dichloromethane / 3.5 h / 20 °C

2: diisobutylaluminium hydride / hexane; dichloromethane / 3.17 h / -40 - 0 °C

3: 1H-imidazole; iodine; triphenylphosphine / tetrahydrofuran / 1 h / 20 °C

4: potassium tert-butylate / tetrahydrofuran / 0.67 h / 0 °C

With 1H-imidazole; potassium tert-butylate; iodine; pyridinium p-toluenesulfonate; diisobutylaluminium hydride; triphenylphosphine; In tetrahydrofuran; hexane; dichloromethane;
DOI:10.1021/ja300565t