(1S,2R)-N-2-amino-1,2-bis(3-methylphenyl)ethylallyl carbamate

Base Information

Chemical Name:(1S,2R)-N-2-amino-1,2-bis(3-methylphenyl)ethylallyl carbamate
CAS No.:1582815-30-2
Molecular Formula:C₂₀H₂₄N₂O₂
Molecular Weight:324.423
Hs Code.:

Synonyms:(1S,2R)-N-2-amino-1,2-bis(3-methylphenyl)ethylallyl carbamate

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Chemical Property of (1S,2R)-N-2-amino-1,2-bis(3-methylphenyl)ethylallyl carbamate

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Technology Process of (1S,2R)-N-2-amino-1,2-bis(3-methylphenyl)ethylallyl carbamate

There total 2 articles about (1S,2R)-N-2-amino-1,2-bis(3-methylphenyl)ethylallyl carbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 15022-08-9
diallylcarbonate

: 117106-34-0
meso-1,2-bis(3-methylphenyl)-1,2-ethanediamine

: 1582815-30-2
(1S,2R)-N-2-amino-1,2-bis(3-methylphenyl)ethylallyl carbamate

: (1R,2S)-N-2-amino-1,2-bis(3-methylphenyl)ethylallyl carbamate

Guidance literature:: With Candida antarctica lipase type A; at 45 ℃; for 62h; Overall yield = 16 %; enantioselective reaction; Inert atmosphere; Enzymatic reaction;
DOI:10.1016/j.tetasy.2014.01.007

Reference yield:

: 620-23-5
m-tolyl aldehyde

: 1582815-30-2
(1S,2R)-N-2-amino-1,2-bis(3-methylphenyl)ethylallyl carbamate

: (1R,2S)-N-2-amino-1,2-bis(3-methylphenyl)ethylallyl carbamate

Guidance literature:: Multi-step reaction with 2 steps

1.1: 3 h / 120 °C

1.2: 12 h / 170 °C

2.1: Candida antarctica lipase type A / 62 h / 45 °C / Inert atmosphere; Enzymatic reaction

With Candida antarctica lipase type A;
DOI:10.1016/j.tetasy.2014.01.007