2,10-diphenyl-6-oxa-2,10-diphosphabicyclo<9.4.0>pentadeca-11(1),12,14-triene

Base Information

Chemical Name:2,10-diphenyl-6-oxa-2,10-diphosphabicyclo<9.4.0>pentadeca-11(1),12,14-triene
CAS No.:72110-13-5
Molecular Formula:C₂₄H₂₆OP₂
Molecular Weight:392.417
Hs Code.:

Synonyms:2,10-diphenyl-6-oxa-2,10-diphosphabicyclo<9.4.0>pentadeca-11(1),12,14-triene

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Chemical Property of 2,10-diphenyl-6-oxa-2,10-diphosphabicyclo<9.4.0>pentadeca-11(1),12,14-triene

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Technology Process of 2,10-diphenyl-6-oxa-2,10-diphosphabicyclo<9.4.0>pentadeca-11(1),12,14-triene

There total 1 articles about 2,10-diphenyl-6-oxa-2,10-diphosphabicyclo<9.4.0>pentadeca-11(1),12,14-triene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 629-36-7
bis(3-chloropropyl)ether

: 38023-29-9
1,2-diphenylphosphinobenzene

: 72110-13-5
2,10-diphenyl-6-oxa-2,10-diphosphabicyclo<9.4.0>pentadeca-11(1),12,14-triene

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; Heating;
DOI:10.1021/ja00521a025

Reference yield: 40.0%

: 72110-13-5
2,10-diphenyl-6-oxa-2,10-diphosphabicyclo<9.4.0>pentadeca-11(1),12,14-triene

: cobalt(II) bromide

: Co⁽²⁺⁾*2Br^(1-)*C₆H₄(P(C₆H₅)(CH₂)3)2O*CHCl₃ = [C₆H₄(P(C₆H₅)(CH₂)3)2O]CoBr₂*CHCl₃

Guidance literature:: In tetrahydrofuran; soln. of ligand was added to Co salt in THF; concn., cooling to -20°C, recrystn. from CHCl3/hexane; elem. anal.;

Reference yield: 20.0%

: cobalt(II) chloride hexahydrate

: 72110-13-5
2,10-diphenyl-6-oxa-2,10-diphosphabicyclo<9.4.0>pentadeca-11(1),12,14-triene

: Co⁽²⁺⁾*2Cl^(1-)*C₆H₄(P(C₆H₅)(CH₂)3)2O= [C₆H₄(P(C₆H₅)(CH₂)3)2O]CoCl₂

Guidance literature:: In ethanol; dichloromethane; soln. of Co salt in EtOH was added to soln. of ligand in CH2Cl2 at roomtemp.; concn. in vac. at room temp.;