2-(2-chloroethyl)-4-(2-acetoxyethyl)-6,7-bis-(2-methoxycarbonylethyl)-1,3,5,8-tetramethyl-γ-acetoxyporphyrin

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Chemical Name:2-(2-chloroethyl)-4-(2-acetoxyethyl)-6,7-bis-(2-methoxycarbonylethyl)-1,3,5,8-tetramethyl-γ-acetoxyporphyrin
CAS No.:87377-84-2
Molecular Formula:C₄₀H₄₅ClN₄O₈
Molecular Weight:745.272
Hs Code.:

Synonyms:2-(2-chloroethyl)-4-(2-acetoxyethyl)-6,7-bis-(2-methoxycarbonylethyl)-1,3,5,8-tetramethyl-γ-acetoxyporphyrin

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Chemical Property of 2-(2-chloroethyl)-4-(2-acetoxyethyl)-6,7-bis-(2-methoxycarbonylethyl)-1,3,5,8-tetramethyl-γ-acetoxyporphyrin

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Technology Process of 2-(2-chloroethyl)-4-(2-acetoxyethyl)-6,7-bis-(2-methoxycarbonylethyl)-1,3,5,8-tetramethyl-γ-acetoxyporphyrin

There total 1 articles about 2-(2-chloroethyl)-4-(2-acetoxyethyl)-6,7-bis-(2-methoxycarbonylethyl)-1,3,5,8-tetramethyl-γ-acetoxyporphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4792-10-3
3-{5-Formyl-2-[5-formyl-3-(2-methoxycarbonyl-ethyl)-4-methyl-1H-pyrrol-2-ylmethyl]-4-methyl-1H-pyrrol-3-yl}-propionic acid methyl ester

: 87377-84-2
2-(2-chloroethyl)-4-(2-acetoxyethyl)-6,7-bis-(2-methoxycarbonylethyl)-1,3,5,8-tetramethyl-γ-acetoxyporphyrin

Guidance literature:: Multi-step reaction with 3 steps

1: 36 percent / sulphuryl chloride / acetic acid / 1 h / Ambient temperature

2: 89 percent / methanesulphonic acid / CH₂Cl₂ / 2 h / Ambient temperature

3: 61 percent / pyridine / 20 °C

With sulfuryl dichloride; methanesulfonic acid; In pyridine; dichloromethane; acetic acid;
DOI:10.1016/S0040-4020(01)88698-1