(3R,4R)-3-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-[(R)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]tetrahydrofuran

Base Information

• Chemical Name: (3R,4R)-3-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-[(R)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]tetrahydrofuran
• CAS No.: 868128-00-1
• Molecular Formula: C₃₄H₃₆O₇
• Molecular Weight: 556.656

Synonyms:(3R,4R)-3-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-[(R)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]tetrahydrofuran

Chemical Property of (3R,4R)-3-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-[(R)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]tetrahydrofuran

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Technology Process of (3R,4R)-3-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-[(R)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]tetrahydrofuran

There total 1 articles about (3R,4R)-3-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-[(R)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]tetrahydrofuran which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

(3R,4R)-3-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]tetrahydrofuran (868127-96-2) → (3R,4R)-3-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-[(R)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]tetrahydrofuran (868128-00-1)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h;

DOI:10.1021/np050089s

Reference yield: 80.0%

(3R,4R)-3-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-[(R)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]tetrahydrofuran (868128-00-1) → (3R,4R)-3-[(S)-(hydroxy)(4-hydroxy-3-methoxyphenyl)methyl]-4-[(R)-(hydroxy)(4-hydroxy-3-methoxyphenyl)methyl]tetrahydrofuran

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; at 20 ℃; for 2h;

DOI:10.1021/np050089s

Reference yield: 78.0%

(3R,4R)-3-[(S)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]-4-[(R)-(4-benzyloxy-3-methoxyphenyl)(hydroxy)methyl]tetrahydrofuran (868128-00-1) → (3R,4R)-3,4-bis(4-benzyloxy-3-methoxybenzoyl)tetrahydrofuran (868128-02-3)

Guidance literature:

With 4 A molecular sieve; pyridinium chlorochromate; In dichloromethane; at 20 ℃; for 16h;

DOI:10.1021/np050089s

upstream raw materials:

(3R,4R)-3-[(S)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]-4-[(R)-(4-benzyloxy-3-methoxyphenyl)(triisopropylsilyloxy)methyl]tetrahydrofuran

Downstream raw materials:

(3R,4R)-3,4-bis(4-benzyloxy-3-methoxybenzoyl)tetrahydrofuran

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