acetylacetonato(22,23,72,73,122,123,172,173-octaphenyltetrapyrazino[b,g,l,q]-5,10,15,20-tetraazaporphyrinato)thulium(III)

Base Information

Chemical Name:acetylacetonato(22,23,72,73,122,123,172,173-octaphenyltetrapyrazino[b,g,l,q]-5,10,15,20-tetraazaporphyrinato)thulium(III)
CAS No.:1127415-17-1
Molecular Formula:C₅H₇O₂*C₇₂H₄₀N₁₆*Tm
Molecular Weight:1397.26
Hs Code.:

Synonyms:acetylacetonato(22,23,72,73,122,123,172,173-octaphenyltetrapyrazino[b,g,l,q]-5,10,15,20-tetraazaporphyrinato)thulium(III)

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Chemical Property of acetylacetonato(22,23,72,73,122,123,172,173-octaphenyltetrapyrazino[b,g,l,q]-5,10,15,20-tetraazaporphyrinato)thulium(III)

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Technology Process of acetylacetonato(22,23,72,73,122,123,172,173-octaphenyltetrapyrazino[b,g,l,q]-5,10,15,20-tetraazaporphyrinato)thulium(III)

There total 1 articles about acetylacetonato(22,23,72,73,122,123,172,173-octaphenyltetrapyrazino[b,g,l,q]-5,10,15,20-tetraazaporphyrinato)thulium(III) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: tris(acetylacetonato)thulium(III)

: 52197-23-6
5,6-diphenyl-pyrazine-2,3-dicarbonitrile

: 1127415-17-1
acetylacetonato(22,23,72,73,122,123,172,173-octaphenyltetrapyrazino[b,g,l,q]-5,10,15,20-tetraazaporphyrinato)thulium(III)

Guidance literature:: With sodium methylate; urea; In benzonitrile; mixt. of 0.66 mmol 5,6-diphenylpyrazine-2,3-dicarbonitrile and 0.16 mmolof metal complex, benzonitrile, 1.6 mmol of urea, catalytical amt. of M eONa heated to 160°C in quartz ampoule and kept at that temp. for1 h; hot filtered; solvent distd. off under vac.; residue purified by column chromy. on silica gel (DMF, 1:1 as eluent); elem. anal.;
DOI:10.1134/S1070363207110175