Technology Process of C73H102O10Si2
There total 19 articles about C73H102O10Si2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
tetrahydrofuran; 1,1-Dibromoethane; N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride; lead(II) chloride; zinc;
In
dichloromethane;
at 65 ℃;
for 4h;
Inert atmosphere;
DOI:10.1021/ja200089f
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: diisobutylaluminium hydride / dichloromethane; toluene / 1.5 h / -78 °C / Inert atmosphere
2.1: di(n-butyl)tin oxide / methanol / 2.5 h / 70 °C / Inert atmosphere
2.2: 12 h / Inert atmosphere
3.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 2 h / 40 °C / Inert atmosphere
3.2: 40 °C / Inert atmosphere
4.1: tetrahydrofuran; 1,1-Dibromoethane; N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride; lead(II) chloride; zinc / dichloromethane / 4 h / 65 °C / Inert atmosphere
With
tetrahydrofuran; 1,1-Dibromoethane; N,N,N,N,-tetramethylethylenediamine; 2,4,6-trichlorobenzoyl chloride; titanium tetrachloride; diisobutylaluminium hydride; di(n-butyl)tin oxide; triethylamine; lead(II) chloride; zinc;
In
tetrahydrofuran; methanol; dichloromethane; toluene;
3.1: Yamaguchi esterification / 3.2: Yamaguchi esterification;
DOI:10.1021/ja200089f
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: di(n-butyl)tin oxide / methanol / 2.5 h / 70 °C / Inert atmosphere
1.2: 12 h / Inert atmosphere
2.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / tetrahydrofuran / 2 h / 40 °C / Inert atmosphere
2.2: 40 °C / Inert atmosphere
3.1: tetrahydrofuran; 1,1-Dibromoethane; N,N,N,N,-tetramethylethylenediamine; titanium tetrachloride; lead(II) chloride; zinc / dichloromethane / 4 h / 65 °C / Inert atmosphere
With
tetrahydrofuran; 1,1-Dibromoethane; N,N,N,N,-tetramethylethylenediamine; 2,4,6-trichlorobenzoyl chloride; titanium tetrachloride; di(n-butyl)tin oxide; triethylamine; lead(II) chloride; zinc;
In
tetrahydrofuran; methanol; dichloromethane;
2.1: Yamaguchi esterification / 2.2: Yamaguchi esterification;
DOI:10.1021/ja200089f