Technology Process of C2HF3O2*C23H30N6O6
There total 7 articles about C2HF3O2*C23H30N6O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: N-ethyl-N,N-diisopropylamine / N,N-dimethyl acetamide / 16 h / 100 °C
2: 4 h
3: magnesium sulfate / N,N-dimethyl acetamide / 80 °C
4: dichloromethane / 20 °C
With
magnesium sulfate; N-ethyl-N,N-diisopropylamine;
In
dichloromethane; N,N-dimethyl acetamide;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: hydrogen / palladium hydroxide on carbon / tetrahydrofuran / 50 °C / 2585.81 Torr
2: potassium carbonate / acetonitrile / 80 °C
3: hydrogenchloride / 1,4-dioxane / 55 °C
4: magnesium sulfate / N,N-dimethyl acetamide / 80 °C
5: dichloromethane / 20 °C
With
hydrogenchloride; hydrogen; magnesium sulfate; potassium carbonate;
palladium hydroxide on carbon;
In
tetrahydrofuran; 1,4-dioxane; dichloromethane; N,N-dimethyl acetamide; acetonitrile;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: potassium carbonate / acetonitrile / 80 °C
2: hydrogenchloride / 1,4-dioxane / 55 °C
3: magnesium sulfate / N,N-dimethyl acetamide / 80 °C
4: dichloromethane / 20 °C
With
hydrogenchloride; magnesium sulfate; potassium carbonate;
In
1,4-dioxane; dichloromethane; N,N-dimethyl acetamide; acetonitrile;