Sodium; 3-{hydroxy-[3-(naphthalen-2-ylmethoxy)-phenyl]-carbamoyl}-propionate

Base Information

Chemical Name:Sodium; 3-{hydroxy-[3-(naphthalen-2-ylmethoxy)-phenyl]-carbamoyl}-propionate
CAS No.:102650-04-4
Molecular Formula:C₂₁H₁₈NO₅*Na
Molecular Weight:387.367
Hs Code.:

Synonyms:Sodium; 3-{hydroxy-[3-(naphthalen-2-ylmethoxy)-phenyl]-carbamoyl}-propionate

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Chemical Property of Sodium; 3-{hydroxy-[3-(naphthalen-2-ylmethoxy)-phenyl]-carbamoyl}-propionate

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Technology Process of Sodium; 3-{hydroxy-[3-(naphthalen-2-ylmethoxy)-phenyl]-carbamoyl}-propionate

There total 5 articles about Sodium; 3-{hydroxy-[3-(naphthalen-2-ylmethoxy)-phenyl]-carbamoyl}-propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 34.0%

: 102650-05-5
4-{[3-(2-naphthalenylmethoxy)phenyl]hydroxyamino}-4-oxobutanoic acid, methyl ester

: 102650-04-4
Sodium; 3-{hydroxy-[3-(naphthalen-2-ylmethoxy)-phenyl]-carbamoyl}-propionate

Guidance literature:: With Claisen's alkali; Ambient temperature;
DOI:10.1021/jm00158a019

Reference yield:

: 554-84-7
meta-nitrophenol

: 102650-04-4
Sodium; 3-{hydroxy-[3-(naphthalen-2-ylmethoxy)-phenyl]-carbamoyl}-propionate

Guidance literature:: Multi-step reaction with 4 steps

1: 65 percent / cesium carbonate, sodium carbonate, potassium iodide / acetone / 72 h / Heating

2: 53 percent / hydrazine hydrate / Pd/C (10percent) / tetrahydrofuran

3: 72 percent / triethylamine / tetrahydrofuran / 1 h / Ambient temperature

4: 34 percent / Claisen's alkali / Ambient temperature

With Claisen's alkali; sodium carbonate; caesium carbonate; hydrazine hydrate; triethylamine; potassium iodide; palladium on activated charcoal; In tetrahydrofuran; acetone;
DOI:10.1021/jm00158a019

Reference yield:

: 79807-83-3
3-(2-naphthalenylmethoxy)nitrobenzene

: 102650-04-4
Sodium; 3-{hydroxy-[3-(naphthalen-2-ylmethoxy)-phenyl]-carbamoyl}-propionate

Guidance literature:: Multi-step reaction with 3 steps

1: 53 percent / hydrazine hydrate / Pd/C (10percent) / tetrahydrofuran

2: 72 percent / triethylamine / tetrahydrofuran / 1 h / Ambient temperature

3: 34 percent / Claisen's alkali / Ambient temperature

With Claisen's alkali; hydrazine hydrate; triethylamine; palladium on activated charcoal; In tetrahydrofuran;
DOI:10.1021/jm00158a019