9-cyclohexylmethyl-1,5-(4-methoxybenzenesulfonyl)-3-methylene-1,5,9-triazacyclododecane

Base Information

Chemical Name:9-cyclohexylmethyl-1,5-(4-methoxybenzenesulfonyl)-3-methylene-1,5,9-triazacyclododecane
CAS No.:1322644-94-9
Molecular Formula:C₃₁H₄₅N₃O₆S₂
Molecular Weight:619.847
Hs Code.:

Synonyms:9-cyclohexylmethyl-1,5-(4-methoxybenzenesulfonyl)-3-methylene-1,5,9-triazacyclododecane

Suppliers and Price of 9-cyclohexylmethyl-1,5-(4-methoxybenzenesulfonyl)-3-methylene-1,5,9-triazacyclododecane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of 9-cyclohexylmethyl-1,5-(4-methoxybenzenesulfonyl)-3-methylene-1,5,9-triazacyclododecane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of 9-cyclohexylmethyl-1,5-(4-methoxybenzenesulfonyl)-3-methylene-1,5,9-triazacyclododecane

There total 6 articles about 9-cyclohexylmethyl-1,5-(4-methoxybenzenesulfonyl)-3-methylene-1,5,9-triazacyclododecane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 881693-79-4
KKD₀₂₅

: 2043-61-0
cyclohexanecarbaldehyde

: 1322644-94-9
9-cyclohexylmethyl-1,5-(4-methoxybenzenesulfonyl)-3-methylene-1,5,9-triazacyclododecane

Guidance literature:: KKD₀₂₅; cyclohexanecarbaldehyde; In ethanol; at 20 ℃; for 1h; Inert atmosphere;

With sodium tetrahydroborate; In ethanol; at 20 ℃; for 24.1667h; Inert atmosphere;
DOI:10.1021/jm2002603

Reference yield:

: N,N'-bis(p-methoxybenzenesulfonyl)bis(3-aminopropyl)benzylamine

: 1322644-94-9
9-cyclohexylmethyl-1,5-(4-methoxybenzenesulfonyl)-3-methylene-1,5,9-triazacyclododecane

Guidance literature:: Multi-step reaction with 3 steps

1.1: sodium hydride / N,N-dimethyl-formamide / Inert atmosphere

1.2: 85 °C / Inert atmosphere

2.1: carbonochloridic acid 1-chloro-ethyl ester / 1,2-dichloro-ethane / Inert atmosphere

2.2: Inert atmosphere; Heating

3.1: ethanol / 1 h / 20 °C / Inert atmosphere

3.2: 24.17 h / 20 °C / Inert atmosphere

With carbonochloridic acid 1-chloro-ethyl ester; sodium hydride; In ethanol; 1,2-dichloro-ethane; N,N-dimethyl-formamide;
DOI:10.1021/jm2002603

Reference yield:

: 881693-71-6
KKD₀₂₃

: 1322644-94-9
9-cyclohexylmethyl-1,5-(4-methoxybenzenesulfonyl)-3-methylene-1,5,9-triazacyclododecane

Guidance literature:: Multi-step reaction with 2 steps

1.1: carbonochloridic acid 1-chloro-ethyl ester / 1,2-dichloro-ethane / Inert atmosphere

1.2: Inert atmosphere; Heating

2.1: ethanol / 1 h / 20 °C / Inert atmosphere

2.2: 24.17 h / 20 °C / Inert atmosphere

With carbonochloridic acid 1-chloro-ethyl ester; In ethanol; 1,2-dichloro-ethane;
DOI:10.1021/jm2002603